(2S)-1-propylpyrrolidine-2-carboxylic acid

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A suspension of 1-n-propyl pyrrolidine-2-carboxylic acid benzyl ester (2.0 g, 8.09 mmol) and 10% Pd on charcoal in methanol (30 mL) was hydrogenated over 12 h. The reaction mixture was filtered through a pad of celite and the filtrate was concentrated (1 g, 77%). The reaction mixture was filtered through a pad of celite the filtrate was concentrated (1 g, 77%)

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A suspension of 1-n-propyl pyrrolidine-2-carboxylic acid benzyl ester (2.0 g, 8.09 mmol) and 10% Pd on charcoal in methanol (30 mL) was hydrogenated over 12 h. The reaction mixture was filtered through a pad of celite and the filtrate was concentrated (1 g, 77%). The reaction mixture was filtered through a pad of celite the filtrate was concentrated (1 g, 77%)

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A suspension of 1-n-propyl pyrrolidine-2-carboxylic acid benzyl ester (2.0 g, 8.09 mmol) and 10% Pd on charcoal in methanol (30 mL) was hydrogenated over 12 h. The reaction mixture was filtered through a pad of celite and the filtrate was concentrated (1 g, 77%). The reaction mixture was filtered through a pad of celite the filtrate was concentrated (1 g, 77%)