sodium;hexadecyl sulfate

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 3.25 g of 2-methoxy-4-(phenylamino)-benzenediazonium bisulfate (Diversitec, Fort Collins, Colo.) in 50 ml of water was neutralized with 0.8 g of sodium bicarbonate in 25 ml water. 3.45 g of sodium hexadecyl sulfate (TCI America, Portland, Oreg., USA) was dissolved in 150 ml of water at 50° C. The solution of the diazonium salt as slowly added to the hexadecyl sulfate solution with stirring. The reaction mixture was stored in the dark at 0-5° C. for 12 hours. The resulting precipitate was filtered off and dried in vacuum. Yield: 5.4 g. dark at 0-5° C. for 12 hours The resulting precipitate was filtered off dried in vacuum

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 3.25 g of 2-methoxy-4-(phenylamino)-benzenediazonium bisulfate (Diverstec, Fort Collins, Colo.) in 50 ml of water was neutralized with 0.8 g of NaHCO3 in 25 ml water, and marked the container with A. 3.45 g of sodium hexadecyl sulfate (TCI America, Portland, Oreg.) was dissolved in 150 ml of water AT 50° C., and marked the container with B. While stirring, solution A was slowly added into solution B and the precipitate was formed after mixing was completed. The reaction mixture was stored in dark at 0-5° C. for 12 hours. The solid was collected by filtration and then dried by vacuum. The yield was 5.4 g. the precipitate was formed after mixing dark at 0-5° C. for 12 hours The solid was collected by filtration dried by vacuum

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 3.25 g of 2-methoxy-4-(phenylamino)-benzenediazonium bisulfate (Diverstec, Fort Collins, Colo.) in 50 ml of water was neutralized with 0.8 g of NaHCO3 in 25 ml water, and marked the container with A. 3.45 g of sodium hexadecyl sulfate (TCI America, Portland, Oreg.) was dissolved in 150 ml of water AT 50° C., and marked the container with B. While stirring, solution A was slowly added into solution B and the precipitate was formed after mixing was completed. The reaction mixture was stored in dark at 0-5° C. for 12 hours. The solid was collected by filtration and then dried by vacuum. The yield was 5.4 g. the precipitate was formed after mixing dark at 0-5° C. for 12 hours The solid was collected by filtration dried by vacuum

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 3.25 g of 2-methoxy-4-(phenylamino)-benzenediazonium bisulfate (Diversitec, Fort Collins, Colo.) in 50 ml of water was neutralized with 0.8 g of sodium bicarbonate in 25 ml water. 3.45 g of sodium hexadecyl sulfate (TCI America, Portland, Oreg., USA) was dissolved in 150 ml of water at 50° C. The solution of the diazonium salt as slowly added to the hexadecyl sulfate solution with stirring. The reaction mixture was stored in the dark at 0-5° C. for 12 hours. The resulting precipitate was filtered off and dried in vacuum. Yield: 5.4 g. dark at 0-5° C. for 12 hours The resulting precipitate was filtered off dried in vacuum

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Glyceryl monostearate containing sodium lauryl sulphate

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Glyceryl monostearate containing sodium lauryl sulphate

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 3.25 g of 2-methoxy-4-(phenylamino)-benzenediazonium bisulfate (Diversitec, Fort Collins, Colo.) in 50 ml of water was neutralized with 0.8 g of sodium bicarbonate in 25 ml water. 3.45 g of sodium hexadecyl sulfate (TCI America, Portland, Oreg., USA) was dissolved in 150 ml of water at 50° C. The solution of the diazonium salt as slowly added to the hexadecyl sulfate solution with stirring. The reaction mixture was stored in the dark at 0–5° C. for 12 hours. The resulting precipitate was filtered off and dried in vacuum. Yield: 5.4 g. dark at 0–5° C. for 12 hours The resulting precipitate was filtered off dried in vacuum

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Glyceryl monostearate containing sodium lauryl sulphate

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 3.25 g of 2-methoxy-4-(phenylamino)-benzenediazonium bisulfate (Diverstec, Fort Collins, Colo.) in 50 ml of water was neutralized with 0.8 g of NaHCO3 in 25 ml water, and marked the container with A. 3.45 g of sodium hexadecyl sulfate (TCI America, Portland, Oreg.) was dissolved in 150 ml of water AT 50° C., and marked the container with B. While stirring, solution A was slowly added into solution B and the precipitate was formed after mixing was completed. The reaction mixture was stored in dark at 0-5° C. for 12 hours. The solid was collected by filtration and then dried by vacuum. The yield was 5.4 g. the precipitate was formed after mixing dark at 0-5° C. for 12 hours The solid was collected by filtration dried by vacuum