2-amino-6-fluorobenzenesulfonamide

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 2-Amino-6-fluoro-benzenesulfonamide (38 mg, 200 μmol) and (E)-2-(4-phenylphenyl)ethenesulfonyl chloride (56 mg, 200 μmol) were dissolved in pyridine (1.5 mL) and the reaction mixture was shaken for 12 h. The solvent was removed in vacuum and the residues were purified by HPLC to give the product (16.6 mg, 19%). The solvent was removed in vacuum the residues were purified by HPLC

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 2-Amino-6-fluoro-benzenesulfonamide (38 mg, 200 μmol) and (E)-2-(4-phenylphenyl)ethenesulfonyl chloride (56 mg, 200 μmol) were dissolved in pyridine (1.5 mL) and the reaction mixture was shaken for 12 h. The solvent was removed in vacuum and the residues were purified by HPLC to give the product (16.6 mg, 19%). The solvent was removed in vacuum the residues were purified by HPLC