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CC(CO[Si](C)(C)C(C)(C)C)O製品情報
1-[tert-butyl(dimethyl)silyl]oxypropan-2-ol (CAS 116286-81-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 13175134
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
11 反応 · 11 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-98e0b147617141ebac410a1b2dfc67a0反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-d10aba08e8de41b687872367f71db78f反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-c7eb00ce43b344cebe6094b1a42d61a0反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-98e0b147617141ebac410a1b2dfc67a0反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-98e0b147617141ebac410a1b2dfc67a0反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of propylene glycol (1.0 g, 13 mmol) in DCM (60.0 mL) was added tert-butyldimethylchlorosilane (2.0 g, 13 mmol) followed by DIPEA (3.2 mL, 18 mmol). The reaction mixture was stirred at ambient temperature for 18 hours. The solution was diluted with ether, washed with saturated aqueous NaHCO3, brine, dried over anhydrous MgSO4, filtered, and concentrated in vacuo to afford the title compound. washed with saturated aqueous NaHCO3, brine dried over anhydrous MgSO4 filtered concentrated in vacuo
ソース ID: ord-51591661a1e145398e734a4d0f0936fb反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of propylene glycol (1.0 g, 13 mmol) in DCM (60.0 mL) was added tert-butyldimethylchlorosilane (2.0 g, 13 mmol) followed by DIPEA (3.2 mL, 18 mmol). The reaction mixture was stirred at ambient temperature for 18 hours. The solution was diluted with ether, washed with saturated aqueous NaHCO3, brine, dried over anhydrous MgSO4, filtered, and concentrated in vacuo to afford the title compound. washed with saturated aqueous NaHCO3, brine dried over anhydrous MgSO4 filtered concentrated in vacuo
ソース ID: ord-51591661a1e145398e734a4d0f0936fb反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-d10aba08e8de41b687872367f71db78f反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-c7eb00ce43b344cebe6094b1a42d61a0反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of propylene glycol (1.0 g, 13 mmol) in DCM (60.0 mL) was added tert-butyldimethylchlorosilane (2.0 g, 13 mmol) followed by DIPEA (3.2 mL, 18 mmol). The reaction mixture was stirred at ambient temperature for 18 hours. The solution was diluted with ether, washed with saturated aqueous NaHCO3, brine, dried over anhydrous MgSO4, filtered, and concentrated in vacuo to afford the title compound. washed with saturated aqueous NaHCO3, brine dried over anhydrous MgSO4 filtered concentrated in vacuo
ソース ID: ord-af268d2303924882ad1b3ae120212e3a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of propylene glycol (1.0 g, 13 mmol) in DCM (60.0 mL) was added tert-butyldimethylchlorosilane (2.0 g, 13 mmol) followed by DIPEA (3.2 mL, 18 mmol). The reaction mixture was stirred at ambient temperature for 18 hours. The solution was diluted with ether, washed with saturated aqueous NaHCO3, brine, dried over anhydrous MgSO4, filtered, and concentrated in vacuo to afford the title compound. washed with saturated aqueous NaHCO3, brine dried over anhydrous MgSO4 filtered concentrated in vacuo
ソース ID: ord-51591661a1e145398e734a4d0f0936fbPubChem References
化合物の公開データベース記録に掲載された情報源です。
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見積依頼
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