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COC(=O)CCCCC(=O)ON1C(=O)CCC1=O製品情報
6-O-(2,5-dioxopyrrolidin-1-yl) 1-O-methyl hexanedioate (CAS 118380-06-6) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 4458286
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-61f2a60045fd461899e3f60ddf7577b4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-b421e2ead8834c3facc6be62830614a1反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-0e4b65e135004351a70e7dc493482219反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-11ded5dc5bf84e10a5c9ac7f08bd70a1反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-6ee06cc338d74b2ebea19761b8727ee9反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-61f2a60045fd461899e3f60ddf7577b4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-6ee06cc338d74b2ebea19761b8727ee9反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-5f655c6ba110436886cd9e450e375530反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 7.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 pg (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-208506fc77e1499ba20693221f23f956反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-b421e2ead8834c3facc6be62830614a1反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-0e4b65e135004351a70e7dc493482219反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of methyl succinimidyl adipate (4.5 g, 17.5 mmol), chlorotrimethylsilane (11.1 ml, 87.5 mmol) and sodium iodide (13.1 g, 87.5 mmol) in 10 ml of acetonitrile was heated at reflux for 12 hours. The mixture was then cooled to room temperature and diluted with ethyl acetate. The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution was colorless. Then it was washed with brine, dried over anhydrous magnesium sulfate, filtered and concentrated to provide 3.2 g (71 percent yield by weight) of adipic acid monosuccinimidyl ester as a white solid. at reflux for 12 hours The reaction mixture was washed repeatedly with 5 percent aqueous sodium bisulfite until the organic solution Then it was washed with brine dried over anhydrous magnesium sulfate filtered concentrated
ソース ID: ord-11ded5dc5bf84e10a5c9ac7f08bd70a1PubChem References
化合物の公開データベース記録に掲載された情報源です。
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