10-bromo-1,1,1-trifluorodecane

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A stirred solution of 1-bromo-10,10,10-trifluorodecane (4.75 g) and triphenylphosphine (4.53 g) in acetonitrile (100 ml) was heated under reflux for 3 days. The solution was evaporated under vacuum and the residue was washed with ether, dissolved in toluene and the solution diluted with ether to give the product as a hygroscopic solid. under reflux for 3 days The solution was evaporated under vacuum the residue was washed with ether dissolved in toluene the solution diluted with ether