N-butyl-3-hydroxy-2,2-dimethylpropanamide

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215d (Method A) from methyl 3-hydroxy-2,2-dimethylpropanoate and n-butyl amine in 100% yield. MS 174 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215d (Method A) from methyl 3-hydroxy-2,2-dimethylpropanoate and n-butyl amine in 100% yield. MS 174 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 197d (Method A) from methyl 3-hydroxy-2,2-dimethylpropanoate and n-butyl amine in 100% yield. MS 174 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 197c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 207c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215d (Method A) from methyl 3-hydroxy-2,2-dimethylpropanoate and n-butyl amine in 100% yield. MS 174 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215d (Method A) from methyl 3-hydroxy-2,2-dimethylpropanoate and n-butyl amine in 100% yield. MS 174 (MH+).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared as in Example 215c from N-butyl-3-hydroxy-2,2-dimethylpropanamide (Example 228c) and 2,6-dinitrobenzonitrile in 66% yield. MS 320 (MH+).