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C1=CC=C(C=C1)C=CCNC2=CC=CC=C2N製品情報
2-N-(3-phenylprop-2-enyl)benzene-1,2-diamine (CAS 130964-01-1) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 2771663
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
11 反応 · 11 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-37c5097d406b4f8480326f67e9b7fb58反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-266e0cf5246844e980eb1d10edff193d反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-37c5097d406b4f8480326f67e9b7fb58反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimethylformamide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure. The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure eluted with chloroform
ソース ID: ord-a7e0d5e171c84e88ae43b3ef41f02629反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimethylformamide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure. The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure eluted with chloroform
ソース ID: ord-a7e0d5e171c84e88ae43b3ef41f02629反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimithylformaide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure The resulting residue eluted with chloroform
ソース ID: ord-fe25518ea9ed4d34b2044f4a465444f9反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-266e0cf5246844e980eb1d10edff193d反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimithylformaide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure The resulting residue eluted with chloroform
ソース ID: ord-fe25518ea9ed4d34b2044f4a465444f9反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimithylformaide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure. The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure eluted with chloroform
ソース ID: ord-b0b86372d756477d9cfc48622dbf0d6f反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimethylformamide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure. The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure eluted with chloroform
ソース ID: ord-a7e0d5e171c84e88ae43b3ef41f02629反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 3.24 g of ortho-phenylenediamine was dissolved in 30 ml of dimithylformaide, to the solution were added 2.07 g of potassium carbonate and 1.52 g of cinnamyl chloride, and the mixture was stirred overnight at a room temperature. After adding 100 ml of water, the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform, and the extract was washed with a saturated sodium chloride aqueous solution, dried over magnesium sulfate and evaporated to remove the solvent under a reduced pressure The resulting residue was applied to a silica gel column and eluted with chloroform, to obtain 2.0 g of the title compound as light brown crystals. the reaction mixture was extracted twice with 100 ml and 50 ml of chloroform the extract was washed with a saturated sodium chloride aqueous solution dried over magnesium sulfate evaporated to remove the solvent under a reduced pressure The resulting residue eluted with chloroform
ソース ID: ord-fe25518ea9ed4d34b2044f4a465444f9PubChem References
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