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CCOC(=O)C1CNCCO1製品情報
ethyl morpholine-2-carboxylate (CAS 135782-25-1) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 15651197
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
8 反応 · 8 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-8d42ce2c14664a76b3058cd82de27d5b反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
ソース ID: ord-3ddb97006a7d4eeab694b2a3cd377a73反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
ソース ID: ord-3ddb97006a7d4eeab694b2a3cd377a73反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
ソース ID: ord-269a8acf6abe4520bcb17149a8afaff3反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-8d42ce2c14664a76b3058cd82de27d5b反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
ソース ID: ord-33ad05b0ab804b288b8aa1dd0e10474b反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
ソース ID: ord-3ddb97006a7d4eeab694b2a3cd377a73反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
ソース ID: ord-269a8acf6abe4520bcb17149a8afaff3PubChem References
化合物の公開データベース記録に掲載された情報源です。
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