N,N'-dibutyloxamide

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: The temperature is brought to 5° C. with an ice-bath and a solution of n-butyl-amine (25 ml, 0.253 mol) in anhydrous methyl alcohol (25 ml) is dripped in. The reaction is exothermic and dripping is adjusted to keep the temperature below 10°-12° C. When all the methyl alcohol solution of the amine has been added, the reaction mixture has a jelly appearance. The temperature is brought to 5° C. with an ice-bath the temperature below 10°-12° C

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: The temperature is brought to 5° C. with an ice-bath and a solution of n-butyl-amine (25 ml, 0.253 mol) in anhydrous methyl alcohol (25 ml) is dripped in. The reaction is exothermic and dripping is adjusted to keep the temperature below 10°-12° C. When all the methyl alcohol solution of the amine has been added, the reaction mixture has a jelly appearance. The temperature is brought to 5° C. with an ice-bath the temperature below 10°-12° C