反応 #1535883
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07078425B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-N-(4-phenyl-butyl)-acetamide-hydrogen chloride salt is stirred with benzophenone imine (12.6 mL, 75 mmol) in CH2Cl2 (200 mL) for 24 h. The organics are then washed with water, dried (MgSO4), and concentrated to provide 2-(diphenylmethylenamino)-N-(4-phenyl-butyl)-acetamide (7) as a white solid which is used without further purification. The organics are then washed with water dried (MgSO4) concentrated
ソース ID: ord-0425835e9f904429b2a1ada31b068d43