1-hexyl-3-phenylthiourea

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared by the method described in Example 1 from N-hexyl-N'-phenylthiourea (3.4 g, 14 mmoles) and acetylenedicarboxylic acid (1.7 g, 14 mmoles). Recrystallization from acetonitrile gave the product (3.0 g), mp 145°-146° C. Prepared by the method Recrystallization from acetonitrile

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Obtained (a) by a procedure analogous to that indicated in Example 1(a), from 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 3-n-hexyl-1-phenylthiourea, or (b) by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-n-hexyl-2-phenyliminothiazolidin-4-ol hydrobromide. Colorless crystals; melting point 234° C. (with decomposition).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Obtained (a) by a procedure analogous to that indicated in Example 1(a), from 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 3-n-hexyl-1-phenylthiourea, or (b) by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-n-hexyl-2-phenyliminothiazolidin-4-ol hydrobromide. Colorless crystals; melting point 234° C. (with decomposition).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared by the method described in Example 1 from N-hexyl-N'-phenylthiourea (3.4 g, 14 mmoles) and acetylenedicarboxylic acid (1.7 g, 14 mmoles). Recrystallization from acetonitrile gave the product (3.0 g), mp 145°-146° C. Prepared by the method Recrystallization from acetonitrile

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Obtained (a) by a procedure analogous to that indicated in Example 1(a), from 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 3-n-hexyl-1-phenylthiourea, or (b) by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-n-hexyl-2-phenyliminothiazolidin-4-ol hydrobromide. Colorless crystals; melting point 234° C. (with decomposition).