01
反応 #3845494
反応式
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関連文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-505ea6bfa76a44beaf6937e637e25a8f2D 化学構造データベース ID 4060908
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SMILES
CCCCCCCCCCNCCO——
製品情報
2-(decylamino)ethanol
2-(decylamino)ethanol (CAS 15196-28-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
CAS番号15196-28-8
データベース ID4060908
分子式—
更新日2023-01-08
想定用途
想定用途
専門的研究・工業用途限定
データベース ID 4060908
計算物性
精密質量—
XLogP—
トポロジカル極性表面積—
水素結合供与体—
水素結合受容体—
回転可能結合—
- IUPAC 名
- —
- InChIKey
- —
- SMILES
- CCCCCCCCCCNCCO
- InChI
- —
安全上の注意
安全性と注記
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
関連反応
12 反応 · 12 文献
02
反応 #3461983
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06962970B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-13053ecaab3f44b3bd5db3ca2a123c8703
反応 #3461982
反応式
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+表示可能な構造データがありません
+表示可能な構造データがありません
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06962970B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-13053ecaab3f44b3bd5db3ca2a123c8704
反応 #3289666
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07351791B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-5c2d11e84f3143b581cce0ef62e83c3605
反応 #2911646
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06949681B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-91ee54bef4f34732a4859ad6625da0c006
反応 #2253447
反応式
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関連文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-505ea6bfa76a44beaf6937e637e25a8f07
反応 #1981154
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07723470B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with 10 (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with 10 (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-ffacfc1d539a4eaf8aa41057464b33a008
反応 #1927283
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07101964B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-a9a00092b7824515ae10ed77ed9a9d9a09
反応 #1927282
反応式
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+表示可能な構造データがありません
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07101964B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-a9a00092b7824515ae10ed77ed9a9d9a10
反応 #1708384
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06392012B1
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65 ° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-952fb4a214454a8db0b52f831480a11e11
反応 #1395940
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08030445B2
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-9ab85a7ae55644058a1b24be46c037c212
反応 #1085725
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06455669B1
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
ソース ID: ord-4e9e7e7bf12a4aa9962579c5b14b83ebPubChem References
公開参考資料
化合物の公開データベース記録に掲載された情報源です。