3-isocyanatopropyl(trimethoxy)silane

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Melt cyclohexanedimethanol in laboratory oven. When melted, take 294.7 g of cyclohexanedimethanol along with 0.11 g dibutyl tin dilaurate and place in a flask at about 35° C. Add 419.5 g of isocyanatopropyltrimethoxysilane over 75 minutes. Then hold for two hours. Cool and empty. at about 35° C Cool