4-bromo-N-[(4-methoxyphenyl)methyl]aniline

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a mixture of (4-bromophenyl)(4-methoxyphenyl)methylamine, 1-1-c, (2 g, 6.8 mmol) in acetonitrile (25 ml) was added BOC2O (1.5 equivalents) and stirred at room temperature for 24 h. The reaction mixture was evaporated to dryness and purified over silica gel (5% MeOH/DCM) to give N-Boc-(4-bromophenyl)(4-methoxyphenyl)methylamine. The reaction mixture was evaporated to dryness purified over silica gel (5% MeOH/DCM)