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2-methyl-1H-pyrrole-3-carbaldehyde (CAS 17619-39-5) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 5324585
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-ed722204d9914c198a25f993c0142a93反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-b9e1f204b69248169d38f5878b43d94d反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-f79920d39bc14c25877443eec3f8f165反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-f79920d39bc14c25877443eec3f8f165反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar operation as in Reference Example 146 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%).
ソース ID: ord-1b4040ea8b244784a73c41d6a3f4df43反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-ed722204d9914c198a25f993c0142a93反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-389a45f5070e40a2a4842c3c925b407d反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-51742964f6c24fae9ef0b3f957608b9f反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-513562b5d66e45dc8744109ff39c9817反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-8a33091c0b1b4e679b9c175d38bbb056反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-a35336974acb4304aebbc3dad4474320反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: By a similar reaction as in Reference Example 44 and using 2-methyl-1H-pyrrole-3-carbaldehyde (1.10 g), sodium hydride (60% in oil, 1.20 g), 15-crown-5 (6.0 mL) and pyridin-3-ylsulfonyl chloride hydrochloride (3.22 g), the title compound was obtained as white crystals (yield 1.10 g, 44%). By a similar reaction as in Reference Example 44
ソース ID: ord-0c951f45b1dc459f9763ed1bcc0b6ad9PubChem References
化合物の公開データベース記録に掲載された情報源です。
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