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BrC1C=CC(=CC=1)CN1CCCCC1製品情報
1-(4-BROMO-BENZYL)-PIPERIDINE (CAS 178162-69-1) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 16495045
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
9 反応 · 9 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-c0b79b41b3834cb98782256884b32605反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-c0b79b41b3834cb98782256884b32605反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-fb29a4bf7a864afcb4d07e5fc67c89d9反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-fb29a4bf7a864afcb4d07e5fc67c89d9反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-fb29a4bf7a864afcb4d07e5fc67c89d9反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-76f6794fd1874c53a2bc6884bb9ff8c0反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-3d2f066ae78c4e5f9f73ff58cffaf0a5反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-5da2efb6be014092b78ce61c208c336e反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 4-bromobenzaldehyde (5 g), piperidine (2.9 mL), and acetic acid (1.5 mL) in DCE (65 mL) was treated with sodium triacetoxyborohydride (6.9 g). After 27 h, the resulting mixture was treated with saturated aqueous sodium bicarbonate (50 mL), and extracted with DCM (2×50 mL). The combined organic phases were dried (magnesium sulfate) and evaporated. Kugelrohr distillation of the residue (160° C., 5 mm Hg) gave the title compound as a pale yellow oil (5.9 g). extracted with DCM (2×50 mL) The combined organic phases were dried (magnesium sulfate) evaporated Kugelrohr distillation of the residue (160° C., 5 mm Hg)
ソース ID: ord-fb29a4bf7a864afcb4d07e5fc67c89d9PubChem References
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