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CC(=O)OCC(C)(C)C1=CC=CC=C1製品情報
(2-methyl-2-phenylpropyl) acetate (CAS 18755-52-7) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 303084
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-688adc34700b4a3a83d64ebb4f08bfce反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-b7afb9c306fb4881bb786340eb4db4f9反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-8e9a249bb124491ba1b37911a333890a反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-c9290e86d35d4fcea96a9534171811cd反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-f0972dc0bd054f8b959b469e5157427e反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-f0972dc0bd054f8b959b469e5157427e反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-b7afb9c306fb4881bb786340eb4db4f9反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-8e9a249bb124491ba1b37911a333890a反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separate the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) separate the organic layer Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-8e9a249bb124491ba1b37911a333890a反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-688adc34700b4a3a83d64ebb4f08bfce反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separte the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-5cfc3a906a1c48469541a3768ba94a02反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Mix methallyl acetate (228 g, 2.0 mol) and benzene (1 L) and cool to 5° C. Add aluminum chloride (266 g, 2.0 mol) over approximately 30 minutes while maintaining the temperature below 10° C. Add, in portions of 50 mL to 80 mL each, to a 5° C. mixture of aluminum chloride (15 g) in benzene (600 mL). After addition is complete, stir at 0-3° C. for ½ hour, pour onto ice (2 kg) and separte the organic layer. Wash with water (2×300 mL), dry (Na2SO4), and distill to give neophyl acetate. Add, in portions of 50 mL to 80 mL each, to a 5° C. After addition pour onto ice (2 kg) Wash with water (2×300 mL) dry (Na2SO4) distill
ソース ID: ord-5cfc3a906a1c48469541a3768ba94a02PubChem References
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