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CNC1CCCCC1O製品情報
2-(methylamino)cyclohexan-1-ol (CAS 20431-83-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 316731
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-4cf607409e79428a874b813e2302093f反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-07a73a5287314e6aa9d57b7837fa9320反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-1c9edf7d50bd46fcb289296b142c0395反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-7e009cbc5f334649bc5db51e386d7ef2反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-4cf607409e79428a874b813e2302093f反応条件: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of (2-hydroxy-cyclohexyl)-carbamic acid ethyl ester (2.06 g, 11.0 mmol, 1.0 eq.) in THF (80 mL) was added LiAlH4 (1.09 g, 28.7 mmol, 2.6 eq.) and the resulting mixture was heated at 65° C. for 2 h. The reaction mixture was cooled to 0° C., quenched with water, and the separated aqueous phase was extracted with 3×EtOAc. The combined organic phase was dried over MgSO4, filtered and concentrated to give 2-methylamino-cyclohexanol (1.19 g, 84%). The reaction mixture was cooled to 0° C. quenched with water the separated aqueous phase was extracted with 3×EtOAc The combined organic phase was dried over MgSO4 filtered concentrated
ソース ID: ord-c31a0b1e22ff43f7a338c88071aa01db反応条件: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of (2-hydroxy-cyclohexyl)-carbamic acid ethyl ester (2.06 g, 11.0 mmol, 1.0 eq.) in THF (80 mL) was added LiAlH4 (1.09 g, 28.7 mmol, 2.6 eq.) and the resulting mixture was heated at 65° C. for 2 h. The reaction mixture was cooled to 0° C., quenched with water, and the separated aqueous phase was extracted with 3×EtOAc. The combined organic phase was dried over MgSO4, filtered and concentrated to give 2-methylamino-cyclohexanol (1.19 g, 84%). The reaction mixture was cooled to 0° C. quenched with water the separated aqueous phase was extracted with 3×EtOAc The combined organic phase was dried over MgSO4 filtered concentrated
ソース ID: ord-c31a0b1e22ff43f7a338c88071aa01db反応条件: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of (2-hydroxy-cyclohexyl)-carbamic acid ethyl ester (2.06 g, 11.0 mmol, 1.0 eq.) in THF (80 mL) was added LiAlH4 (1.09 g, 28.7 mmol, 2.6 eq.) and the resulting mixture was heated at 65° C. for 2 h. The reaction mixture was cooled to 0° C., quenched with water, and the separated aqueous phase was extracted with 3×EtOAc. The combined organic phase was dried over MgSO4, filtered and concentrated to give 2-methylamino-cyclohexanol (1.19 g, 84%). The reaction mixture was cooled to 0° C. quenched with water the separated aqueous phase was extracted with 3×EtOAc The combined organic phase was dried over MgSO4 filtered concentrated
ソース ID: ord-c31a0b1e22ff43f7a338c88071aa01db反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-07a73a5287314e6aa9d57b7837fa9320反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-1c9edf7d50bd46fcb289296b142c0395反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-7e009cbc5f334649bc5db51e386d7ef2反応条件: temp:65.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of (2-hydroxy-cyclohexyl)-carbamic acid ethyl ester (2.06 g, 11.0 mmol, 1.0 eq.) in THF (80 mL) was added LiAlH4 (1.09 g, 28.7 mmol, 2.6 eq.) and the resulting mixture was heated at 65° C. for 2 h. The reaction mixture was cooled to 0° C., quenched with water, and the separated aqueous phase was extracted with 3×EtOAc. The combined organic phase was dried over MgSO4, filtered and concentrated to give 2-methylamino-cyclohexanol (1.19 g, 84%). The reaction mixture was cooled to 0° C. quenched with water the separated aqueous phase was extracted with 3×EtOAc The combined organic phase was dried over MgSO4 filtered concentrated
ソース ID: ord-ee435313d2df42daaa0add3299571340PubChem References
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