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C1=CC=C(C(=C1)CC(C(=O)N)N)F製品情報
2-amino-3-(2-fluorophenyl)propanamide (CAS 208655-11-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 22346608
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
7 反応 · 7 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-032fe7ec07a0430291eac5ac4dd7cc78反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-3-(2-fluorophenyl)propionamide was added carefully to a chilled (5°) mixture of LAH (1.0 g, 26.3 mmol) and 20 ml THF under argon. The reaction was then heated at reflux for 10 hrs. The reaction was cooled to 5° C. and carefully treated with Na2SO4.10 H2O. The resulting mixture was stirred for 18 hrs, then filtered to remove the solids. The filtrate was concentrated in vacuo to give an amber oil. MS (m/z): 169 (M+H)+; C9H13FN2 requir. 168.19 a chilled The reaction was then heated at reflux for 10 hrs filtered to remove the solids The filtrate was concentrated in vacuo to give an amber oil
ソース ID: ord-29fe5172f9d94884869e0ed43b282c11反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-3-(2-fluorophenyl)propionamide was added carefully to a chilled (5°) mixture of LAH (1.0 g, 26.3 mmol) and 20 ml THF under argon. The reaction was then heated at reflux for 10 hrs. The reaction was cooled to 5° C. and carefully treated with Na2SO4.10 H2O. The resulting mixture was stirred for 18 hrs, then filtered to remove the solids. The filtrate was concentrated in vacuo to give an amber oil. MS (m/z): 169 (M+H)+; C9H13FN2 requir. 168.19 a chilled The reaction was then heated at reflux for 10 hrs filtered to remove the solids The filtrate was concentrated in vacuo to give an amber oil
ソース ID: ord-29fe5172f9d94884869e0ed43b282c11反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-3-(2-fluorophenyl)propionamide was added carefully to a chilled (5°) mixture of LAH (1.0 g, 26.3 mmol) and 20 ml THF under argon. The reaction was then heated at reflux for 10 hrs. The reaction was cooled to 5° C. and carefully treated with Na2SO4.10 H2O. The resulting mixture was stirred for 18 hrs, then filtered to remove the solids. The filtrate was concentrated in vacuo to give an amber oil. MS (m/z): 169 (M+H)+; C9H13FN2 requir. 168.19 a chilled The reaction was then heated at reflux for 10 hrs filtered to remove the solids The filtrate was concentrated in vacuo to give an amber oil
ソース ID: ord-29fe5172f9d94884869e0ed43b282c11反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-3-(2-fluorophenyl)propionamide was added carefully to a chilled (50°) mixture of LAH (1.0 g, 26.3 mmol) and 20 ml THF under argon. The reaction was then heated at reflux for 10 hrs. The reaction was cooled to 5° C. and carefully treated with Na2SO4.10H2O. The resulting mixture was stirred for 18 hrs, then filtered to remove the solids. The filtrate was concentrated in vacuo to give an amber oil. MS (m/z): 169 (M+H)+; C9H13FN2 requir. 168.19. a chilled The reaction was then heated at reflux for 10 hrs filtered to remove the solids The filtrate was concentrated in vacuo to give an amber oil
ソース ID: ord-7177bc8e9d6b4c96b1271afd6ee3f475反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-3-(2-fluorophenyl)propionamide was added carefully to a chilled (5°) mixture of LAH (1.0 g, 26.3 mmol) and 20 ml THF under argon. The reaction was then heated at reflux for 10 hrs. The reaction was cooled to 5° C. and carefully treated with Na2SO4.10 H2O. The resulting mixture was stirred for 18 hrs, then filtered to remove the solids. The filtrate was concentrated in vacuo to give an amber oil. MS (m/z): 169 (M+H)+; C9H13FN2 requir. 168.19 a chilled The reaction was then heated at reflux for 10 hrs filtered to remove the solids The filtrate was concentrated in vacuo to give an amber oil
ソース ID: ord-9f6770dec1e143eaacef0b3e0e5b3803反応条件: temp:5.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 2-Amino-3-(2-fluorophenyl)propionamide was added carefully to a chilled (5°) mixture of LAH (1.0 g, 26.3 mmol) and 20 ml THF under argon. The reaction was then heated at reflux for 10 hrs. The reaction was cooled to 5° C. and carefully treated with Na2SO4.10 H2O. The resulting mixture was stirred for 18 hrs, then filtered to remove the solids. The filtrate was concentrated in vacuo to give an amber oil. MS (m/z): 169 (M+H)+; C9H13FN2 requir. 168.19 a chilled The reaction was then heated at reflux for 10 hrs filtered to remove the solids The filtrate was concentrated in vacuo to give an amber oil
ソース ID: ord-29fe5172f9d94884869e0ed43b282c11PubChem References
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