1,3-dihexylthiourea

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared by the method described in Example 1 from N,N'-dihexylthiourea (114.2 g, 468 mmoles) and acetylenedicarboxylic acid (53.4 g, 468 mmoles). Recrystallization from acetonitrile gave the product (50.4 g) mp 66°-69° C. Prepared by the method Recrystallization from acetonitrile

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared by the method described in Example 1 from N,N'-dihexylthiourea (114.2 g, 468 mmoles) and acetylenedicarboxylic acid (53.4 g, 468 mmoles). Recrystallization from acetonitrile gave the product (50.4 g) mp 66°-69° C. Prepared by the method Recrystallization from acetonitrile

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-di-n-hexyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diethyl ether and the remaining oil was treated with cyclohexane. the end product was precipitated with diethyl ether the remaining oil was treated with cyclohexane

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-di-n-hexyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diethyl ether and the remaining oil was treated with cyclohexane. Colorless, amorphous solid body: decomposition beginning at 75° C., γ C=N 1615 cm-1. the end product was precipitated with diethyl ether the remaining oil was treated with cyclohexane beginning at 75° C.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Prepared by the method described in Example 1 from N,N'-dihexylthiourea (114.2 g, 468 mmoles) and acetylenedicarboxylic acid (53.4 g, 468 mmoles). Recrystallization from acetonitrile gave the product (50.4 g) mp 66°-69° C. Prepared by the method Recrystallization from acetonitrile

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-di-n-hexyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diethyl ether and the remaining oil was treated with cyclohexane. the end product was precipitated with diethyl ether the remaining oil was treated with cyclohexane