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CCCCCCCCCCCCCCCC1=CC=CC=C1製品情報
pentadecylbenzene (CAS 2131-18-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 16476
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
6 反応 · 6 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-a9ec0de59d824bfaa49401447a2eb934反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A 500-ml-three-necked round-bottomed flask, with an efficient cooling was charged with aluminium chloride (5.82 g, 43.67 mmol) and dichloromethane (100 ml). Acetyl chloride (3.42 g, 43.67 mmol) was added to the vigorously stirred reaction mixture over a period of 15 minutes. Pentadecyl benzene (10 g, 34.66 mmol) was added over a period of 30 minutes; the clear solution was stirred at 0° C. for 2 hours and allowed to warm to room temperature. The reaction mixture was poured in ice and extracted with dichloromethane (3×100 ml), the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml), dried over sodium sulfate and the solvent was evaporated to obtain 4-acetyl pentadecyl benzene as a low melting faint yellow solid. The yield was 10 g (87% of theoretical). A 500-ml-three-necked round-bottomed flask, with an efficient cooling to warm to room temperature The reaction mixture was poured in ice extracted with dichloromethane (3×100 ml) the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml) dried over sodium sulfate the solvent was evaporated
ソース ID: ord-abea354b382545379932525665d4a8a5反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A 500-ml-three-necked round-bottomed flask, with an efficient cooling was charged with aluminium chloride (5.82 g, 43.67 mmol) and dichloromethane (100 ml). Acetyl chloride (3.42 g, 43.67 mmol) was added to the vigorously stirred reaction mixture over a period of 15 minutes. Pentadecyl benzene (10 g, 34.66 mmol) was added over a period of 30 minutes; the clear solution was stirred at 0° C. for 2 hours and allowed to warm to room temperature. The reaction mixture was poured in ice and extracted with dichloromethane (3×100 ml), the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml), dried over sodium sulfate and the solvent was evaporated to obtain 4-acetyl pentadecyl benzene as a low melting faint yellow solid. The yield was 10 g (87% of theoretical). A 500-ml-three-necked round-bottomed flask, with an efficient cooling to warm to room temperature The reaction mixture was poured in ice extracted with dichloromethane (3×100 ml) the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml) dried over sodium sulfate the solvent was evaporated
ソース ID: ord-abea354b382545379932525665d4a8a5反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A 500-ml-three-necked round-bottomed flask, with an efficient cooling was charged with aluminium chloride (5.82 g, 43.67 mmol) and dichloromethane (100 ml). Acetyl chloride (3.42 g, 43.67 mmol) was added to the vigorously stirred reaction mixture over a period of 15 minutes. Pentadecyl benzene (10 g, 34.66 mmol) was added over a period of 30 minutes; the clear solution was stirred at 0° C. for 2 hours and allowed to warm to room temperature. The reaction mixture was poured in ice and extracted with dichloromethane (3×100 ml), the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml), dried over sodium sulfate and the solvent was evaporated to obtain 4-acetyl pentadecyl benzene as a low melting faint yellow solid. The yield was 10 g (87% of theoretical). A 500-ml-three-necked round-bottomed flask, with an efficient cooling to warm to room temperature The reaction mixture was poured in ice extracted with dichloromethane (3×100 ml) the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml) dried over sodium sulfate the solvent was evaporated
ソース ID: ord-abea354b382545379932525665d4a8a5反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-a9ec0de59d824bfaa49401447a2eb934反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A 500-ml-three-necked round-bottomed flask, with an efficient cooling was charged with aluminium chloride (5.82 g, 43.67 mmol) and dichloromethane (100 ml). Acetyl chloride (3.42 g, 43.67 mmol) was added to the vigorously stirred reaction mixture over a period of 15 minutes. Pentadecyl benzene (10 g, 34.66 mmol) was added over a period of 30 minutes; the clear solution was stirred at 0° C. for 2 hours and allowed to warm to room temperature. The reaction mixture was poured in ice and extracted with dichloromethane (3×100 ml), the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml), dried over sodium sulfate and the solvent was evaporated to obtain 4-acetyl pentadecyl benzene as a low melting faint yellow solid. The yield was 10 g (87% of theoretical). A 500-ml-three-necked round-bottomed flask, with an efficient cooling to warm to room temperature The reaction mixture was poured in ice extracted with dichloromethane (3×100 ml) the combined organic layers was washed with 1 N hydrochloric acid (2×30 ml) and water (3×50 ml) dried over sodium sulfate the solvent was evaporated
ソース ID: ord-abea354b382545379932525665d4a8a5PubChem References
化合物の公開データベース記録に掲載された情報源です。