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COC1=CC=CC(=C1OS(=O)(=O)C2=CC=CC=C2)C=O製品情報
(2-formyl-6-methoxyphenyl) benzenesulfonate (CAS 2426-85-9) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 233765
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
7 反応 · 7 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-dcdc979aa53d4109b6d0e99b70ecda1b反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: o-Vanillin (350 g, 2.3 mols) was added to a solution of NaOH (166 g, 4.15 mols) in 2 1 water. Benzenesulfonyl chloride (485 g, 2.74 mols) was added to the slurry at 20°-25° C. over 1 hour. The solid which formed was collected on a filter, washed with 2 1 water, and redissolved in CH2Cl2. That solution was dried (MgSO4) and evaporated to a slurry. The solid was collected on a filter, the filtrate was further evaporated and filtered. The solid was washed with MeOH and dried in vacuo to afford the desired product, (511 g, 81.4%), mp 120°-122° C. The solid which formed was collected on a filter washed with 2 1 water redissolved in CH2Cl2 That solution was dried (MgSO4) evaporated to a slurry The solid was collected on a filter the filtrate was further evaporated filtered The solid was washed with MeOH dried in vacuo
ソース ID: ord-431ea247edda41e18083483885f4b972反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: o-Vanillin (350 g, 2.3 mols) was added to a solution of NaOH (166 g, 4.15 mols) in 2 l water. Benzenesulfonyl chloride (485 g, 2.74 mols) was added to the slurry at 20°-25° C. over 1 hour. The solid which formed was collected on a filter, washed with 2 l water, and redissolved in CH2Cl2. That solution was dried (MgSO4) and evaporated to a slurry. The solid was collected on a filter, the filtrate was further evaporated and filtered. The solid was washed with MeOH and dried in vacuo to afford the desired product, (511 g, 81.4%), mp 120°-122° C. The solid which formed was collected on a filter washed with 2 l water redissolved in CH2Cl2 That solution was dried (MgSO4) evaporated to a slurry The solid was collected on a filter the filtrate was further evaporated filtered The solid was washed with MeOH dried in vacuo
ソース ID: ord-e99e9095bfe44ccdbd3965e13ac09b0d反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: o-Vanillin (350 g, 2.3 mols) was added to a solution of NaOH (166 g, 4.15 mols) in 2 l water. Benzenesulfonyl chloride (485 g, 2.74 mols) was added to the slurry at 20°-25° C. over 1 hour. The solid which formed was collected on a filter, washed with 2 l water, and redissolved in CH2Cl2. That solution was dried (MgSO4) and evaporated to a slurry. The solid was collected on a filter, the filtrate was further evaporated and filtered. The solid was washed with MeOH and dried in vacuo to afford the desired product, (511 g, 81.4%), mp 120°-122° C. The solid which formed was collected on a filter washed with 2 l water redissolved in CH2Cl2 That solution was dried (MgSO4) evaporated to a slurry The solid was collected on a filter the filtrate was further evaporated filtered The solid was washed with MeOH dried in vacuo
ソース ID: ord-e99e9095bfe44ccdbd3965e13ac09b0d反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-dcdc979aa53d4109b6d0e99b70ecda1b反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: o-Vanillin (350 g, 2.3 mols) was added to a solution of NaOH (166 g, 4.15 mols) in 2 1 water. Benzenesulfonyl chloride (485 g, 2.74 mols) was added to the slurry at 20°-25° C. over 1 hour. The solid which formed was collected on a filter, washed with 2 1 water, and redissolved in CH2Cl2. That solution was dried (MgSO4) and evaporated to a slurry. The solid was collected on a filter, the filtrate was further evaporated and filtered. The solid was washed with MeOH and dried in vacuo to afford the desired product, (511 g, 81.4%), mp 120°-122° C. The solid which formed was collected on a filter washed with 2 1 water redissolved in CH2Cl2 That solution was dried (MgSO4) evaporated to a slurry The solid was collected on a filter the filtrate was further evaporated filtered The solid was washed with MeOH dried in vacuo
ソース ID: ord-431ea247edda41e18083483885f4b972反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: o-Vanillin (350 g, 2.3 mols) was added to a solution of NaOH (166 g, 4.15 mols) in 2 l water. Benzenesulfonyl chloride (485 g, 2.74 mols) was added to the slurry at 20°-25° C. over 1 hour. The solid which formed was collected on a filter, washed with 2 l water, and redissolved in CH2Cl2. That solution was dried (MgSO4) and evaporated to a slurry. The solid was collected on a filter, the filtrate was further evaporated and filtered. The solid was washed with MeOH and dried in vacuo to afford the desired product, (511 g, 81.4%), mp 120°-122° C. The solid which formed was collected on a filter washed with 2 l water redissolved in CH2Cl2 That solution was dried (MgSO4) evaporated to a slurry The solid was collected on a filter the filtrate was further evaporated filtered The solid was washed with MeOH dried in vacuo
ソース ID: ord-e99e9095bfe44ccdbd3965e13ac09b0dPubChem References
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