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CCOC(=O)CCCCCCCl製品情報
ethyl 7-chloroheptanoate (CAS 26040-65-3) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 529988
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
11 反応 · 11 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-7645b856c6a842dabe138b2a8dfb198e反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.2 g. of NaH (80% suspension in mineral oil), 9.8 g. of 1-(3-chlorophenyl)-benzimidazolin-2-one (produced in usual manners by subjecting N-(3-chlorophenyl)-o-phenylene diamine to reaction of phosgene), 80 cc. of DMF, 7.7 g. of 7-chloroenanthic acid ethyl ester and 1.2 g. of NaJ. The product is produced
ソース ID: ord-e9c878b2428847d899354acc8b732023反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.9 g. of NaH (80% suspension in mineral oil), 13.2 g. of 1-phenylbenzimidazolin-2-one (produced in usual manner by subjecting N-phenyl-o-phenylenediamine to reaction with phosgene), 120 cc. of DMF, 12.1 g. of 7-chloroenanthic acid ethyl ester and 1.9 g. of NaJ. Eluant in chromatographic purification: hexane/ethylacetate. The product is produced Eluant in chromatographic purification
ソース ID: ord-5de6ee76530c498fbd32795bab90ea10反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.2 g. of NaH (80% suspension in mineral oil), 9.8 g. of 1-(3-chlorophenyl)-benzimidazolin-2-one (produced in usual manners by subjecting N-(3-chlorophenyl)-o-phenylene diamine to reaction of phosgene), 80 cc. of DMF, 7.7 g. of 7-chloroenanthic acid ethyl ester and 1.2 g. of NaJ. The product is produced
ソース ID: ord-e9c878b2428847d899354acc8b732023反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.2 g. of NaH (80% suspension in mineral oil), 9.8 g. of 1-(3-chlorophenyl)-benzimidazolin-2-one (produced in usual manners by subjecting N-(3-chlorophenyl)-o-phenylene diamine to reaction of phosgene), 80 cc. of DMF, 7.7 g. of 7-chloroenanthic acid ethyl ester and 1.2 g. of NaJ. The product is produced
ソース ID: ord-e9c878b2428847d899354acc8b732023反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.9 g. of NaH (80% suspension in mineral oil), 13.2 g. of 1-phenylbenzimidazolin-2-one (produced in usual manner by subjecting N-phenyl-o-phenylenediamine to reaction with phosgene), 120 cc. of DMF, 12.1 g. of 7-chloroenanthic acid ethyl ester and 1.9 g. of NaJ. Eluant in chromatographic purification: hexane/ethylacetate. The product is produced Eluant in chromatographic purification
ソース ID: ord-5de6ee76530c498fbd32795bab90ea10反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.9 g. of NaH (80% suspension in mineral oil), 13.2 g. of 1-phenylbenzimidazolin-2-one (produced in usual manner by subjecting N-phenyl-o-phenylenediamine to reaction with phosgene), 120 cc. of DMF, 12.1 g. of 7-chloroenanthic acid ethyl ester and 1.9 g. of NaJ. Eluant in chromatographic purification: hexane/ethylacetate. The product is produced Eluant in chromatographic purification
ソース ID: ord-5de6ee76530c498fbd32795bab90ea10反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is obtained as described in example 1 from 2.1 g of NaH (80% suspension in mineral oil), 18.5 g of 1-ethyl-4.5-diphenyl-4-imidazolin-2-one, 140 cc. of DMF, 13.5 g of 7-chloroenanthic acid ethyl ester and 2.1 g of NaJ. The product is obtained
ソース ID: ord-5c9d7533d6a6403cad679228344b1a0a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is obtained as described in example 1 from 1.35 g NaJ (80% suspension in mineral oil), 12.2 g of 1-(4-chlorophenyl)-5-phenyl-4-imidazolin-2-one, 100 cc. of DMF, 8.7 g of 7-chloroenanthic acid ethyl ester and 1.35 g of NaJ. Eluant in chromatographic purification: hexane/ethyl acetate. The product is obtained Eluant in chromatographic purification
ソース ID: ord-70babe5b36c84ee19e60180bfe43ff58反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.2 g. of NaH (80% suspension in mineral oil), 9.8 g. of 1-(3-chlorophenyl)-benzimidazolin-2-one (produced in usual manners by subjecting N-(3-chlorophenyl)-o-phenylene diamine to reaction of phosgene), 80 cc. of DMF, 7.7 g. of 7-chloroenanthic acid ethyl ester and 1.2 g. of NaJ. The product is produced
ソース ID: ord-e9c878b2428847d899354acc8b732023反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The product is produced as described in example 1 from 1.9 g. of NaH (80% suspension in mineral oil), 13.2 g. of 1-phenylbenzimidazolin-2-one (produced in usual manner by subjecting N-phenyl-o-phenylenediamine to reaction with phosgene), 120 cc. of DMF, 12.1 g. of 7-chloroenanthic acid ethyl ester and 1.9 g. of NaJ. Eluant in chromatographic purification: hexane/ethylacetate. The product is produced Eluant in chromatographic purification
ソース ID: ord-5de6ee76530c498fbd32795bab90ea10PubChem References
化合物の公開データベース記録に掲載された情報源です。