tert-butyl N-[(1R,2R)-2-aminocyclopropyl]carbamate

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Starting from dimethyl trans-1,2-cyclopropanedicarboxylate, trans-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride may be prepared and purified analogously to cis-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride (see 58.4). M.p: 200-202° C. may be prepared purified analogously to cis-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride (see 58.4)

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Starting from dimethyl trans-1,2-cyclopropanedicarboxylate, trans-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride may be prepared and purified analogously to cis-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride (see 58.4). M.p: 200-202° C. may be prepared purified analogously to cis-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride (see 58.4)

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Starting from dimethyl trans-1,2-cyclopropanedicarboxylate, trans-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride may be prepared and purified analogously to cis-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride (see 58.4). M.p: 200-202° C. may be prepared purified analogously to cis-N-tert-butyloxycarbonyl-1,2-cyclopropanediamin hydrochloride (see 58.4)