butane-1,4-disulfonyl chloride

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 2,5-diamino-1,4-benzenedithiol vapor in the condensing chamber 2 was adiabatically expanded, and the introduced modified particles (35) were exposed thereto for 18 minutes. Consequently, a further polymerization reaction between 1,4-butanedisulfonyl chloride and 2,5-diamino-1,4-benzenedithiol took place on the surface of the modified particles (35), forming a film of 1,4-butanedisulfonylchloride-2,5-diamino-1,4-benzenedithiol co-polymer.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 2,5-diamino-1,4-benzenedithiol vapor in the condensing chamber 2 was adiabatically expanded, and the introduced modified particles (35) were exposed thereto for 18 minutes. Consequently, a further polymerization reaction between 1,4-butanedisulfonyl chloride and 2,5-diamino-1,4-benzenedithiol took place on the surface of the modified particles (35), forming a film of 1,4-butanedisulfonylchloride-2,5-diamino-1,4-benzenedithiol co-polymer.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 1,4-butanedisulfonyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 15 minutes. Consequently, 1,4-butanedisulfonyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between 1,4-butanedisulfonyl chloride condensed on the surface of the base particles and 6-amino-2-mercaptobenzothiazole contained therein, forming a film of 6-amino-2-mercaptobenzothiazole-1,4-butanedisulfonyl chloride co-polymer on the surface of the base particles. A polymerization reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 1,4-butanedisulfonyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 15 minutes. Consequently, 1,4-butanedisulfonyl chloride condensed on the surface of the base particles. A polymerization reaction, using as a catalyst triethylamine contained in the base particles, took place between 1,4-butanedisulfonyl chloride condensed on the surface of the base particles and 6-amino-2-mercaptobenzothiazole contained therein, forming a film of 6-amino-2-mercaptobenzothiazole-1,4-butanedisulfonyl chloride co-polymer on the surface of the base particles. A polymerization reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 1,4-butanedisulfonyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 8 minutes. Consequently, a polymerization reaction between 2,5-diamino-1,4-benzenedithiol and 1,4-butanedisulfonyl chloride took place on the surface of the base particles, forming a film of 2,5-diamino-1,4-benzenedithiol-1,4-butanedisulfonyl chloride co-polymer.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, in the mixing section 22, the vapor atmosphere of 1,10-diaminodecane was cooled, and the introduced base particles were exposed thereto for 5 minutes. Consequently, a polymerization reaction took place on the surface of the base particles between 1,4-butanedisulfonyl chloride and 1,10-diaminodecane, forming a film of 1,4-butanedisulfonylchloride-1,10-diaminodecane co-polymer. Consequently, a polymerization reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, in the mixing section 22, the vapor atmosphere of 1,10-diaminodecane was cooled, and the introduced base particles were exposed thereto for 5 minutes. Consequently, a polymerization reaction took place on the surface of the base particles between 1,4-butanedisulfonyl chloride and 1,10-diaminodecane, forming a film of 1,4-butanedisulfonylchloride-1,10-diaminodecane co-polymer. Consequently, a polymerization reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 5 minutes. Consequently, a polymerization reaction took place on the surface of the base particles between 1,6-diaminohexane and 1,4-butanedisulfonyl chloride, forming a film of 1,6-diaminohexane-1,4-butanedisulfonyl chloride co-polymer. The base particles, along with helium gas, were cooled Consequently, a polymerization reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 1,6-diaminohexane vapor in the condensing chamber 2 was adiabatically expanded, and the introduced modified particles (26) were exposed thereto for 2 minutes. Consequently, a further polymerization reaction between 1,4-butanedisulfonyl chloride and 1,6-diaminohexane took place on the surface of the modified particles (26), forming a film of 1,4-butanedisulfonylchloride-1,6-diaminohexane co-polymer.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Next, the 1,6-diaminohexane vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 3 minutes. Consequently, a polymerization reaction between 1,4-butanedisulfonyl chloride and 1,6-diaminohexane took place on the surface of the base particles, forming a film of 1,4-butanedisulfonylchloride-1,6-diaminohexane co-polymer.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction, using as a catalyst triethylenediamine contained in the base particles, took place on the surface of the base particles between di(2-mercaptoethyl)ether and 1,4-butanedisulfonyl chloride, forming a film of di(2-mercaptoethyl)ether-1,4-butanedisulfonyl chloride co-polymer. The base particles, along with helium gas, were cooled Consequently, a polymerization reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction, using as a catalyst triethylenediamine contained in the base particles, took place on the surface of the base particles between di(2-mercaptoethyl)ether and 1,4-butanedisulfonyl chloride, forming a film of di(2-mercaptoethyl)ether-1,4-butanedisulfonyl chloride co-polymer. The base particles, along with helium gas, were cooled Consequently, a polymerization reaction