4-ethylsulfanylaniline

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 15, 1-[p-(ethylthio)phenyl]-1H-tetrazole (prepared from p-ethylthioaniline by the method of Example 2) is treated with sodium azide and concentrated sulfuric acid to give the S-ethyl-S-[p-(1H-tetrazole-1-yl)-phenyl]sulfoximine.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 15, 1-[p-(ethylthio)phenyl]-1H-tetrazole (prepared from p-ethylthioaniline by the method of Example 2) is treated with sodium azide and concentrated sulfuric acid to give the S-ethyl-S-[p-(1H-tetrazole-1-yl)-phenyl]sulfoximine.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-ethylthioaniline as starting materials, the title compound was obtained as a yellow powder (yield 56%).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-ethylthioaniline as starting materials, the title compound was obtained as a yellow powder (yield 56%).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 15, 1-[p-(ethylthio)phenyl]-1H-tetrazole (prepared from p-ethylthioaniline by the method of Example 2) is treated with sodium azide and concentrated sulfuric acid to give the S-ethyl-S-[p-(1H-tetrazole-1-yl)-phenyl]sulfoximine.

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-ethylthioaniline as starting materials, the title compound was obtained as a yellow powder (yield 56%).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-ethylthioaniline as starting materials, the title compound was obtained as a yellow powder (yield 56%).

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 15, 1-[p-(ethylthio)phenyl]-1H-tetrazole (prepared from p-ethylthioaniline by the method of Example 2) is treated with sodium azide and concentrated sulfuric acid to give the S-ethyl-S-[p-(1H-tetrazole-1-yl)-phenyl]sulfoximine.