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CCOCC1=CC=C(O1)Br製品情報
2-bromo-5-(ethoxymethyl)furan (CAS 35901-20-3) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 59332580
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
7 反応 · 7 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-981f3eac3bc0471ea5d70db2e2f3d4b5反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Sodium hydride (95%, 19 mg, 0.75 mmol) was diluted in dry DMF (0.5 mL) and cooled to 0° C. A solution of (5-bromo-2-furanyl)methanol (120 mg, 0.68 mmol) was added, and the mixture was stirred for 5 minutes. Ethyl iodide (117 mg, 0.75 mmol) was added, and the mixture was stirred at it overnight. The reaction mixtures were quenched by the careful addition of water, then extracted with diethyl ether. The combined organics were dried and concentrated. The residue was purified by flash chromatography, eluting with 10% EtOAc/hexanes. The desired fractions were combined and concentrated to afford the title compound. the mixture was stirred at it overnight The reaction mixtures were quenched by the careful addition of water extracted with diethyl ether The combined organics were dried concentrated The residue was purified by flash chromatography eluting with 10% EtOAc/hexanes concentrated
ソース ID: ord-8549bd640e984336ab3297e886e98be6反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Sodium hydride (95%, 19 mg, 0.75 mmol) was diluted in dry DMF (0.5 mL) and cooled to 0° C. A solution of (5-bromo-2-furanyl)methanol (120 mg, 0.68 mmol) was added, and the mixture was stirred for 5 minutes. Ethyl iodide (117 mg, 0.75 mmol) was added, and the mixture was stirred at rt overnight. The reaction mixtures were quenched by the careful addition of water, then extracted with diethyl ether. The combined organics were dried and concentrated. The residue was purified by flash chromatography, eluting with 10% EtOAc/hexanes. The desired fractions were combined and concentrated to afford the title compound. the mixture was stirred at rt overnight The reaction mixtures were quenched by the careful addition of water extracted with diethyl ether The combined organics were dried concentrated The residue was purified by flash chromatography eluting with 10% EtOAc/hexanes concentrated
ソース ID: ord-f7df9f7d135a4c298f9e3806d15e1e6a反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Sodium hydride (95%, 19 mg, 0.75 mmol) was diluted in dry DMF (0.5 mL) and cooled to 0° C. A solution of (5-bromo-2-furanyl)methanol (120 mg, 0.68 mmol) was added, and the mixture was stirred for 5 minutes. Ethyl iodide (117 mg, 0.75 mmol) was added, and the mixture was stirred at it overnight. The reaction mixtures were quenched by the careful addition of water, then extracted with diethyl ether. The combined organics were dried and concentrated. The residue was purified by flash chromatography, eluting with 10% EtOAc/hexanes. The desired fractions were combined and concentrated to afford the title compound. the mixture was stirred at it overnight The reaction mixtures were quenched by the careful addition of water extracted with diethyl ether The combined organics were dried concentrated The residue was purified by flash chromatography eluting with 10% EtOAc/hexanes concentrated
ソース ID: ord-8549bd640e984336ab3297e886e98be6反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-981f3eac3bc0471ea5d70db2e2f3d4b5反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Sodium hydride (95%, 19 mg, 0.75 mmol) was diluted in dry DMF (0.5 mL) and cooled to 0° C. A solution of (5-bromo-2-furanyl)methanol (120 mg, 0.68 mmol) was added, and the mixture was stirred for 5 minutes. Ethyl iodide (117 mg, 0.75 mmol) was added, and the mixture was stirred at rt overnight. The reaction mixtures were quenched by the careful addition of water, then extracted with diethyl ether. The combined organics were dried and concentrated. The residue was purified by flash chromatography, eluting with 10% EtOAc/hexanes. The desired fractions were combined and concentrated to afford the title compound. the mixture was stirred at rt overnight The reaction mixtures were quenched by the careful addition of water extracted with diethyl ether The combined organics were dried concentrated The residue was purified by flash chromatography eluting with 10% EtOAc/hexanes concentrated
ソース ID: ord-f7df9f7d135a4c298f9e3806d15e1e6a反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Sodium hydride (95%, 19 mg, 0.75 mmol) was diluted in dry DMF (0.5 mL) and cooled to 0° C. A solution of (5-bromo-2-furanyl)methanol (120 mg, 0.68 mmol) was added, and the mixture was stirred for 5 minutes. Ethyl iodide (117 mg, 0.75 mmol) was added, and the mixture was stirred at it overnight. The reaction mixtures were quenched by the careful addition of water, then extracted with diethyl ether. The combined organics were dried and concentrated. The residue was purified by flash chromatography, eluting with 10% EtOAc/hexanes. The desired fractions were combined and concentrated to afford the title compound. the mixture was stirred at it overnight The reaction mixtures were quenched by the careful addition of water extracted with diethyl ether The combined organics were dried concentrated The residue was purified by flash chromatography eluting with 10% EtOAc/hexanes concentrated
ソース ID: ord-8549bd640e984336ab3297e886e98be6PubChem References
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