反応 #3960697
関連文献 (1)
openreactiondata ↗doi:10.1002/anie.201611536
反応条件: temp:120.01; pressure:0.00; stir:
実験手順: Prepared from 2-fluoro-N,N-dimethylaniline (1g, 27.8 mg, 0.200 mmol, 1.00 equiv) and catBH (36.0 mg, 0.300 mmol, 1.50 equiv) according to GP 1. The title compound was purified by flash column chromatography using cyclohexane/EtOAc/Et3N (30/1/1) as eluent to afford 3g (22.2 mg, 42%) as a white solid.
ソース ID: ord-c97bc2351f1641abbf2646050cc1f606