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C#CCOCCl製品情報
3-(chloromethoxy)prop-1-yne (CAS 40308-66-5) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 12241341
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-8b0d3b76c5d949e29497764cce420e2a反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-e27cea3db06e47b0a9d514c8d5ac589f反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-928edf10e5af46e7a697292bb89bfe29反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-8b0d3b76c5d949e29497764cce420e2a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 0.6 g of N-methoxybenzenesulfonamide was dissolved in 10 ml of acetonitrile, and 0.44 g of potassium carbonate and 0.34 g of chloromethylpropargyl ether were added thereto in this order. The mixture was stirred at room temperature for 4 hours. After completion of the reaction, water was added to the reaction solution, and the mixture was extracted with ethyl acetate. The extract was dried, concentrated, and purified by silica gel column chromatography to obtain 0.7 g of N-methoxy-N-propargyloxymethylbenzenesulfonamide. was added to the reaction solution the mixture was extracted with ethyl acetate The extract was dried concentrated purified by silica gel column chromatography
ソース ID: ord-8a7f1a41a70a4d3db418869aba312fea反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 0.6 g of N-methoxybenzamide was dissolved in 10 ml of acetonitrile, and 0.55 g of potassium carbonate and 0.42 g of chloromethylpropargyl ether were added thereto in this order. The mixture was stirred at room temperature for 3 hours. After completion of the reaction, water was added to the reaction solution, and the mixture was extracted with ethyl acetate. The extract was dried, concentrated and purified by silica gel column chromatography to obtain 0.8 g of N-methoxy-N-propargyloxymethylbenzamide. was added to the reaction solution the mixture was extracted with ethyl acetate The extract was dried concentrated purified by silica gel column chromatography
ソース ID: ord-78a2d25f14b9434b93e8ef7743620d47反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 0.37 g of sodium hydride (60% in oil) was suspended in 10 ml of tetrahydrofuran, and 0.8 g of methyl N-methoxycarbamate and 0.96 g of chloromethylpropargyl ether were added thereto in this order while being cooled with ice. The mixture was heat-refluxed for 1 hour. After completion of the reaction, water was added to the reaction solution, and the mixture was extracted with ethyl acetate. The extract was dried, concentrated and purified by silica gel column chromatography to obtain 1.0 g of methyl N-methoxy-N-propargyloxymethylcarbamate. in this order while being cooled with ice The mixture was heat-refluxed for 1 hour was added to the reaction solution the mixture was extracted with ethyl acetate The extract was dried concentrated purified by silica gel column chromatography
ソース ID: ord-b317ab1e31f1484d8c7fa6fc2ad9a7be反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-e27cea3db06e47b0a9d514c8d5ac589f反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-928edf10e5af46e7a697292bb89bfe29反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 0.6 g of N-methoxybenzenesulfonamide was dissolved in 10 ml of acetonitrile, and 0.44 g of potassium carbonate and 0.34 g of chloromethylpropargyl ether were added thereto in this order. The mixture was stirred at room temperature for 4 hours. After completion of the reaction, water was added to the reaction solution, and the mixture was extracted with ethyl acetate. The extract was dried, concentrated, and purified by silica gel column chromatography to obtain 0.7 g of N-methoxy-N-propargyloxymethylbenzenesulfonamide. was added to the reaction solution the mixture was extracted with ethyl acetate The extract was dried concentrated purified by silica gel column chromatography
ソース ID: ord-8a7f1a41a70a4d3db418869aba312fea反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 0.6 g of N-methoxybenzamide was dissolved in 10 ml of acetonitrile, and 0.55 g of potassium carbonate and 0.42 g of chloromethylpropargyl ether were added thereto in this order. The mixture was stirred at room temperature for 3 hours. After completion of the reaction, water was added to the reaction solution, and the mixture was extracted with ethyl acetate. The extract was dried, concentrated and purified by silica gel column chromatography to obtain 0.8 g of N-methoxy-N-propargyloxymethylbenzamide. was added to the reaction solution the mixture was extracted with ethyl acetate The extract was dried concentrated purified by silica gel column chromatography
ソース ID: ord-78a2d25f14b9434b93e8ef7743620d47反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 0.37 g of sodium hydride (60% in oil) was suspended in 10 ml of tetrahydrofuran, and 0.8 g of methyl N-methoxycarbamate and 0.96 g of chloromethylpropargyl ether were added thereto in this order while being cooled with ice. The mixture was heat-refluxed for 1 hour. After completion of the reaction, water was added to the reaction solution, and the mixture was extracted with ethyl acetate. The extract was dried, concentrated and purified by silica gel column chromatography to obtain 1.0 g of methyl N-methoxy-N-propargyloxymethylcarbamate. in this order while being cooled with ice The mixture was heat-refluxed for 1 hour was added to the reaction solution the mixture was extracted with ethyl acetate The extract was dried concentrated purified by silica gel column chromatography
ソース ID: ord-b317ab1e31f1484d8c7fa6fc2ad9a7bePubChem References
化合物の公開データベース記録に掲載された情報源です。