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C1=COC(=C1)CNC(=O)CCl製品情報
2-chloro-N-(furan-2-ylmethyl)acetamide (CAS 40914-13-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 720922
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
9 反応 · 9 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-b479acb552034d01b197d963c532f7a4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-579f141a799349e98a55b521e785a4e5反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-579f141a799349e98a55b521e785a4e5反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwiseso that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-5bde5c864fc84686a5c88f89ebfe68fd反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, addition funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, addition funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-579f141a799349e98a55b521e785a4e5反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: N-Furfurylchloroacetamide was prepared by adding 20.0 g. (0.206 mole) furfuryl amine in sufficient toluene to make a 15% solution to a 500 ml. three neck round bottom flask equipped with magnetic stir bar, additional funnel, and cooling bath and then adding 36 ml. of 20% sodium hydroxide. The mixture was cooled to 0°-5° C. and chloroacetyl chloride was added dropwise so that the reaction temperature was maintained at 5°-10° C. After the addition, a solid deposited on the walls of the flask. It was recrystallized from ether as a light tan solid. Yield was 85%. by adding 20.0 g three neck round bottom flask equipped with magnetic stir bar, additional funnel cooling bath adding 36 ml The mixture was cooled to 0°-5° C. was maintained at 5°-10° C After the addition It was recrystallized from ether as a light tan solid
ソース ID: ord-dfd57f5b61284c5bb698f76d5a2e50f4PubChem References
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