1-dodecoxydodecane

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 185 g of glycerol epichlorhydrin are reacted with 1 mole, i.e., 186 g of dodecanol at 75°-80° C in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 185 g of glycerol epichlorhydrin are reacted with 1 mole, i.e., 186 g of dodecanol at 75°-80° C in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75-80° C in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75°-80° C. in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75°-80° C. in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75°-80° C. in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

反応条件: temp:125.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: After placing 390 parts by weight of n-dodecanol into a reaction vessel and heating to 125° C., one part by weight of p-toluene sulfonic acid as a catalyst was added to the solution, and then the pressure in the vessel was reduced to 5-10 mmHg. Separately, 100 parts by weight of anhydrous crystalline cyclotetrasaccharide, obtained by the method in Example B-3, was suspended in 130 parts by weight of n-dodecanol. The suspension was added into the above vessel drop by drop in a flow rate of 2.3 parts by weight/min with taking a time of 100 min for the reaction. Successively, the reactant was neutralized with aqueous sodium carbonate solution, and cyclotetrasaccharide dodecyl ether was obtained by evaporating residual alcohol. The suspension was added into the above vessel drop by drop in a flow rate of 2.3 parts by weight/min a time of 100 min for the reaction

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: MES (Dojindo Laboratories); EMSE (Daito Chemix Corporation); 4-aminoantipyrine (Saikyo Kasei), CEBP-M (enzyme having an activity of lipoprotein lipase; Asahi Kasei Corporation); GYK-301 (glycerol kinase; Toyobo Co., Ltd.); GPOM (glycerol 3-phosphate oxidase; Asahi Kasei Corporation), catalase (Sigma), peroxidase (Toyobo Co., Ltd.), sodium azide (Kanto Chemicals Co., Inc.), Emulgen B66 (Kao Corporation), Newcol 610 (Nippon Nyukazai Co., Ltd.), Newcol 2608F (Nippon Nyukazai Co., Ltd.), New Calgen GP120 (Takemoto Oil & Fat, Co. Ltd.), NIKKOL R1020 (Nikko Chemicals Co., Ltd.), Emulgen A60 (Kao Corporation), BLAUNON DSP12.5 (Aoki Oil Industrial Co., Ltd.), HI-TENOL N08 (Daichi Kogyo Co., Ltd.), Emulgen L40 (Kao Corporation), Newcol 707SF (Nippon Nyukazai Co., Ltd.), Wondersurf S1400 (Aoki Oil Industrial Co., Ltd.), New Calgen E150 (Takemoto Oil & Fat, Co. Ltd.), Sodium cholate (Acros), Emulgen 909 (POE nonylphenyl ether HLB 12.4; Kao Corporation), Emulmin NL70 (POE lauryl ether HLB 12.4; Sanyo Chemicals Industries, Ltd.).