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C=CCNS(=O)(=O)C1=CC=CC=C1製品情報
N-prop-2-enylbenzenesulfonamide (CAS 50487-70-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 257467
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
8 反応 · 8 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-1f7e696c201049c5834a1c618279d3d4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
ソース ID: ord-f92623c3bd7e4863a1d855ef6cbe29e6反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
ソース ID: ord-f92623c3bd7e4863a1d855ef6cbe29e6反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
ソース ID: ord-e34992c041d64e4f88ecfe12dc444722反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
ソース ID: ord-e34992c041d64e4f88ecfe12dc444722反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-1f7e696c201049c5834a1c618279d3d4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
ソース ID: ord-f92623c3bd7e4863a1d855ef6cbe29e6反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: 1.97 g (0.01 mole) of N-allylbenzenesulfonamide was added to 0.58 g (0.012 mole) of 50% sodium hydride in 15 ml of dry N,N-dimethylformamide. The mixture was stirred at room temperature for 30 minutes to react them. To the resulting sodium salt was added 2.10 g (0.012 mole) of α-methyl-2-chlorobenzyl chloride. The mixture was stirred at room temperature for 1 hour. The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added. The resulting oil layer was extracted with benzene. The benzene layer was dried over anhydrous magnesium sulfate, concentrated, and purified by silica gel chromatography to afford the final product. The final product is designated as compound No. 89 in Table 2, and its melting point and elemental analysis values are shown in Table 2. to react them The mixture was stirred at room temperature for 1 hour The N,N-dimethyl formamide was distilled off under reduced pressure, and cold water was added The resulting oil layer was extracted with benzene The benzene layer was dried over anhydrous magnesium sulfate concentrated purified by silica gel chromatography
ソース ID: ord-e34992c041d64e4f88ecfe12dc444722PubChem References
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