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CC1=CC=CC=C1OCCCBr製品情報
1-(3-bromopropoxy)-2-methylbenzene (CAS 50912-60-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 1622574
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-30fac245f1c54d2ca889c7f7f64dd602反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-41dd943e724a40caab03332b679ada70反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-e99a4bd4f61c471bb12dcba39eb93aa6反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-30fac245f1c54d2ca889c7f7f64dd602反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-41dd943e724a40caab03332b679ada70反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0447 g, 0.152 mmol) and 3-bromopropyl 2-methylphenyl ether (0.0934 g, 0.407 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0586 g, 76.5%). EI-MS m/z 442(M+) Rt (2.17 min). were reacted
ソース ID: ord-b179aba746e14b939745b04f064e833f反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0447 g, 0.152 mmol) and 3-bromopropyl 2-methylphenyl ether (0.0934 g, 0.407 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0586 g, 76.5%). EI-MS m/z 442(M+) Rt (2.17 min). were reacted
ソース ID: ord-b179aba746e14b939745b04f064e833f反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of 2-methylphenol (0.0954 g, 0.924 mmol) in acetonitrile (4 mL) was added 1,3-dibromopropane (1.00 mL, 9.85 mmol) followed by Cs2CO3 (0.469 g, 1.44 mmol). The reaction mixture was stirred for 24 h and then concentrated under vacuum. The resulting residue was treated with H2O (4 mL) and extracted with DCM (8 mL). The organic layer was dried through a phase separator and concentrated under vacuum. The residue was taken up in DMSO and purified by preparatory HPLC (without TFA) to give the title compound (0.0934 g, 44.1%). EI-MS Rt (2.45 min). concentrated under vacuum The resulting residue was treated with H2O (4 mL) extracted with DCM (8 mL) The organic layer was dried through a phase separator concentrated under vacuum purified by preparatory HPLC (without TFA)
ソース ID: ord-c1c3893d431a425d9a2c06d74a113c51反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-e99a4bd4f61c471bb12dcba39eb93aa6反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0447 g, 0.152 mmol) and 3-bromopropyl 2-methylphenyl ether (0.0934 g, 0.407 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0586 g, 76.5%). EI-MS m/z 442 (M+) Rt (2.17 min). were reacted
ソース ID: ord-5efd47ad1f2e45a1a3dbbc1acac02c03反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of 2-methylphenol (0.0954 g, 0.924 mmol) in acetonitrile (4 mL) was added 1,3-dibromopropane (1.00 mL, 9.85 mmol) followed by Cs2CO3 (0.469 g, 1.44 mmol). The reaction mixture was stirred for 24 h and then concentrated under vacuum. The resulting residue was treated with H2O (4 mL) and extracted with DCM (8 mL). The organic layer was dried through a phase separator and concentrated under vacuum. The residue was taken up in DMSO and purified by preparatory HPLC (without TFA) to give the title compound (0.0934 g, 44.1%). EI-MS Rt (2.45 min). concentrated under vacuum The resulting residue was treated with H2O (4 mL) extracted with DCM (8 mL) The organic layer was dried through a phase separator concentrated under vacuum purified by preparatory HPLC (without TFA)
ソース ID: ord-9994cdda74974740bd7062a32c85b6e2反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0447 g, 0.152 mmol) and 3-bromopropyl 2-methylphenyl ether (0.0934 g, 0.407 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0586 g, 76.5%). EI-MS m/z 442 (M+) Rt (2.17 min). were reacted
ソース ID: ord-ad435cb8353d40af980c156c878fc99bPubChem References
化合物の公開データベース記録に掲載された情報源です。
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