DIETHYL 1-TETRADECANEPHOSPHONATE

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 100 g (590 mmol) of triethyl phosphite and 164 g (590 mmol) of 1-bromotetradecane are heated on a column connected to a descending condenser. Bromoethane distills out at a bath temperature of 170° C.; the mixture is then distilled under high vacuum, resulting in the product of boiling point 145° C./0.03 mmHg which is pure by 1H NMR. connected to a descending condenser Bromoethane distills out at a bath temperature of 170° C. the mixture is then distilled under high vacuum resulting in the product of boiling point 145° C./0.03 mmHg which

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 100 g (590 mmol) of triethyl phosphite and 164 g (590 mmol) of 1-bromotetradecane are heated on a column connected to a descending condenser. Bromoethane distills out at a bath temperature of 170° C.; the mixture is then distilled under high vacuum, resulting in the product of boiling point 145° C./0.03 mmHg which is pure by 1H NMR. connected to a descending condenser Bromoethane distills out at a bath temperature of 170° C. the mixture is then distilled under high vacuum resulting in the product of boiling point 145° C./0.03 mmHg which