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CSCC(=O)C1=CC=CC=C1製品情報
2-methylsulfanyl-1-phenylethanone (CAS 5398-93-6) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 220651
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
7 反応 · 7 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-5d51bb3b207546d0b1de202b21f2f9e8反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 21.4 g of bromoacetophenone is added to 90 ml of ethanol at 0° C., followed by slow addition of a solution of 5 g of sodium thiomethoxide in 25 ml of water. The reaction medium is stirred for one hour at 0° C. and then for 2 hours at room temperature, and is subsequently poured on to 500 ml of ice-water and extracted with twice 200 ml of ethyl ether. The ether phases are combined and washed with saturated aqueous sodium chloride, dried over anhydrous sodium sulphate and then evaporated to dryness. The residue is distilled to give 2-(methylthio)acetophenone. for 2 hours at room temperature extracted with twice 200 ml of ethyl ether washed with saturated aqueous sodium chloride dried over anhydrous sodium sulphate evaporated to dryness The residue is distilled
ソース ID: ord-25bbb6eb87ea4be780a3f08b72b6d6de反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 21.4 g of bromoacetophenone is added to 90 ml of ethanol at 0° C., followed by slow addition of a solution of 5 g of sodium thiomethoxide in 25 ml of water. The reaction medium is stirred for one hour at 0° C. and then for 2 hours at room temperature, and is subsequently poured on to 500 ml of ice-water and extracted with twice 200 ml of ethyl ether. The ether phases are combined and washed with saturated aqueous sodium chloride, dried over anhydrous sodium sulphate and then evaporated to dryness. The residue is distilled to give 2-(methylthio)acetophenone. for 2 hours at room temperature extracted with twice 200 ml of ethyl ether washed with saturated aqueous sodium chloride dried over anhydrous sodium sulphate evaporated to dryness The residue is distilled
ソース ID: ord-25bbb6eb87ea4be780a3f08b72b6d6de反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 21.4 g of bromoacetophenone is added to 90 ml of ethanol at 0° C., followed by slow addition of a solution of 5 g of sodium thiomethoxide in 25 ml of water. The reaction medium is stirred for one hour at 0° C. and then for 2 hours at room temperature, and is subsequently poured on to 500 ml of ice-water and extracted with twice 200 ml of ethyl ether. The ether phases are combined and washed with saturated aqueous sodium chloride, dried over anhydrous sodium sulphate and then evaporated to dryness. The residue is distilled to give 2-(methylthio)acetophenone. for 2 hours at room temperature extracted with twice 200 ml of ethyl ether washed with saturated aqueous sodium chloride dried over anhydrous sodium sulphate evaporated to dryness The residue is distilled
ソース ID: ord-25bbb6eb87ea4be780a3f08b72b6d6de反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-5d51bb3b207546d0b1de202b21f2f9e8反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 21.4 g of bromoacetophenone is added to 90 ml of ethanol at 0° C., followed by slow addition of a solution of 5 g of sodium thiomethoxide in 25 ml of water. The reaction medium is stirred for one hour at 0° C. and then for 2 hours at room temperature, and is subsequently poured on to 500 ml of ice-water and extracted with twice 200 ml of ethyl ether. The ether phases are combined and washed with saturated aqueous sodium chloride, dried over anhydrous sodium sulphate and then evaporated to dryness. The residue is distilled to give 2-(methylthio)acetophenone. for 2 hours at room temperature extracted with twice 200 ml of ethyl ether washed with saturated aqueous sodium chloride dried over anhydrous sodium sulphate evaporated to dryness The residue is distilled
ソース ID: ord-9cb2e58379a54ab7be109f0728a7778e反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A solution of 21.4 g of bromoacetophenone is added to 90 ml of ethanol at 0° C., followed by slow addition of a solution of 5 g of sodium thiomethoxide in 25 ml of water. The reaction medium is stirred for one hour at 0° C. and then for 2 hours at room temperature, and is subsequently poured on to 500 ml of ice-water and extracted with twice 200 ml of ethyl ether. The ether phases are combined and washed with saturated aqueous sodium chloride, dried over anhydrous sodium sulphate and then evaporated to dryness. The residue is distilled to give 2-(methylthio)acetophenone. for 2 hours at room temperature extracted with twice 200 ml of ethyl ether washed with saturated aqueous sodium chloride dried over anhydrous sodium sulphate evaporated to dryness The residue is distilled
ソース ID: ord-25bbb6eb87ea4be780a3f08b72b6d6dePubChem References
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