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CCOC(=O)NC1CCCC1製品情報
ethyl N-cyclopentylcarbamate (CAS 54915-64-9) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 4193626
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
11 反応 · 11 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-a73ba837da49461088c0aff04c67ac95反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-a73ba837da49461088c0aff04c67ac95反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-4b5757e07a2f4064ad30c10a9ffc3afb反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-4b5757e07a2f4064ad30c10a9ffc3afb反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-4b5757e07a2f4064ad30c10a9ffc3afb反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-ca6aed742fe14b7dac439effce0674d1反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-ca6aed742fe14b7dac439effce0674d1反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-f774ed5ac10b4dd18e16f0b685b89b80反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-f774ed5ac10b4dd18e16f0b685b89b80反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-f774ed5ac10b4dd18e16f0b685b89b80反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: To a solution of cyclopentylamine (5.8 mL, 59 mmol, 1.0 eq.) in CH2Cl2 (250 mL) at room temperature was added ethylchloroformate (7.3 mL, 1.3 eq.) followed by an aqueous solution of K2CO3 (37 g in 500 mL of H2O). The mixture was stirred vigorously for 1 h. The separated aqueous layer was extracted twice with CH2Cl2. The combined organic layers were dried over MgSO4, filtered and concentrated to give cyclopentyl-carbamic acid ethyl ester (9.6 g, 88%). The separated aqueous layer was extracted twice with CH2Cl2 The combined organic layers were dried over MgSO4 filtered concentrated
ソース ID: ord-4b5757e07a2f4064ad30c10a9ffc3afbPubChem References
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