N'-dodecylpropane-1,3-diamine

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 33, but starring with N-dodecyl-1,3-propanediamine and cyclohexanone, the tide compound is produced; IR nmax (neat) 3292, 2925, 2854, 2810, 1466, 1450, 1367, 1130 and 721 cm-1. (PLA2) the tide compound is produced

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 121 parts of N-dodecylpropanediyl diamine were dissolved in 80 parts of toluene and 98 parts of maleic acid anhydride added at 50° to 60° C. After stirring for 30 minutes at a temperature of 50° to 60° C., the toluene was distilled off under reduced pressure at 50° to 60° C. 221 parts of the crude N-dodecyl-N,N'-propanediyl bis-maleamic acid ##STR9## were obtained. added at 50° to 60° C the toluene was distilled off under reduced pressure at 50° to 60° C

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 121 parts of N-dodecylpropanediyl diamine were dissolved in 80 parts of toluene and 98 parts of maleic acid anhydride added at 50° to 60° C. After stirring for 30 minutes at a temperature of 50° to 60° C., the toluene was distilled off under reduced pressure at 50° to 60° C. 221 parts of the crude N-dodecyl-N,N'-propanediyl bis-maleamic acid ##STR9## were obtained. added at 50° to 60° C the toluene was distilled off under reduced pressure at 50° to 60° C

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 33, but starring with N-dodecyl-1,3-propanediamine and cyclohexanone, the tide compound is produced; IR nmax (neat) 3292, 2925, 2854, 2810, 1466, 1450, 1367, 1130 and 721 cm-1. (PLA2) the tide compound is produced

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 33, but starring with N-dodecyl-1,3-propanediamine and cyclohexanone, the tide compound is produced; IR nmax (neat) 3292, 2925, 2854, 2810, 1466, 1450, 1367, 1130 and 721 cm-1. (PLA2) the tide compound is produced

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: 121 parts of N-dodecylpropanediyl diamine were dissolved in 80 parts of toluene and 98 parts of maleic acid anhydride added at 50° to 60° C. After stirring for 30 minutes at a temperature of 50° to 60° C., the toluene was distilled off under reduced pressure at 50° to 60° C. 221 parts of the crude N-dodecyl-N,N'-propanediyl bis-maleamic acid ##STR9## were obtained. added at 50° to 60° C the toluene was distilled off under reduced pressure at 50° to 60° C

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Into an apparatus similar to that in Example 1, were charged 242.1 g (1 mole) of N-dodecyl-1,3-propylenediamine and 130.1 g (1 mole) of ethyl acetoacetate. At 150° to 160° C., 18 g of water and 46 g of ethanol were distilled off to obtain 1-dodecyl-4-methyl-3,6,7,8-tetrahydro-1,5-diazocin-2-one. At 150° to 160° C., 18 g of water and 46 g of ethanol were distilled off

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Into an apparatus similar to that in Example 1, were charged 242.1 g (1 mole) of N-dodecyl-1,3-propylenediamine and 130.1 g (1 mole) of ethyl acetoacetate. At 150° to 160° C., 18 g of water and 46 g of ethanol were distilled off to obtain 1-dodecyl-4-methyl-3,6,7,8-tetrahydro-1,5-diazocin-2-one. At 150° to 160° C., 18 g of water and 46 g of ethanol were distilled off

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 33, but starting with N-dodecyl-1,3-propanediamine and cyclohexanone, the title compound is produced; IR nmax (neat) 3292, 2925, 2854, 2810, 1466, 1450, 1367, 1130 and 721 cm-1. (PLA2)

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Following the general procedure of Example 33, but starting with N-dodecyl-1,3-propanediamine and cyclohexanone, the title compound is produced; IR νmax (neat) 3292, 2925, 2854, 2810, 1466, 1450, 1367, 1130 and 721 cm-1. (PLA2)