反応 #1177050
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04005103
反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The procedure of Example IX using 24.3 g of 1-cyclopropyl-3-(p-chlorophenyl)prop-2-en-1-one, 11 ml of nitroethane and 1.5 g of sodium in 120 ml of methanol, gives 25 g of 1-cyclopropyl-3-(p-chlorophenyl)-4-nitropentanone as an oily residue which is used in the crude state for the remainder of the operations.
ソース ID: ord-94feced6d85d474f956a8137a8b47f6c