octadeca-9,12,15-trienoyl chloride

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a solution of 1.000 g of 9,12,15-octadecatrienoic acid in 20 ml of dry chloroform at room temperature was added in the atmosphere of argon 0.50 ml of oxalyl chloride. The mixture was reacted for 2 hours. From the reaction mixture were removed the chloroform and the remaining oxalyl chloride by distillation. The 9,12,15-octadecatrienoyl chloride thus produced was again dissolved in 2 ml of dry chloroform. The mixture was reacted for 2 hours From the reaction mixture were removed the chloroform the remaining oxalyl chloride by distillation

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a solution of 1.000 g of 9,12,15-octadecatrienoic acid in 20 ml of dry chloroform at room temperature was added in the atmosphere of argon 0.50 ml of oxalyl chloride. The mixture was reacted for 2 hours. From the reaction mixture were removed the chloroform and the remaining oxalyl chloride by distillation. The 9,12,15-octadecatrienoyl chloride thus produced was again dissolved in 2 ml of dry chloroform. The mixture was reacted for 2 hours From the reaction mixture were removed the chloroform the remaining oxalyl chloride by distillation

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a solution of 1.000 g of 9,12,15-octadecatrienoic acid in 20 ml of dry chloroform at room temperature was added in the atmosphere of argon 0.50 ml of oxalyl chloride. The mixture was reacted for 2 hours. From the reaction mixture were removed the chloroform and the remaining oxalyl chloride by distillation. The 9,12,15-octadecatrienoyl chloride thus produced was again dissolved in 2 ml of dry chloroform. The mixture was reacted for 2 hours From the reaction mixture were removed the chloroform the remaining oxalyl chloride by distillation

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a solution of 834 mg of 9,12,15-octadecatrienic acid in 8 ml of dry chloroform was added 0.4 ml of oxalyl chloride under argon at room temperature. The mixture was reacted for 2 hours. From the reaction mixture were removed the chloroform and the remaining oxalyl chloride by distillation under reduced pressure to give 9,12,15-octadecatrienoyl chloride, which was then dissolved in 6 ml of dry chloroform. The mixture was reacted for 2 hours From the reaction mixture were removed the chloroform the remaining oxalyl chloride by distillation under reduced pressure

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a solution of 834 mg of 9,12,15-octadecatrienoic acid in 8 ml of dry chloroform was added 0.4 ml of oxalyl chloride under argon at room temperature. The mixture was reacted for 2 hours. From the reaction mixture were removed the chloroform and the remaining oxalyl chloride by distillation under reduced pressure to give 9,12,15-octadecatrienoyl chloride, which was then dissolved in 6 ml of dry chloroform. The mixture was reacted for 2 hours From the reaction mixture were removed the chloroform the remaining oxalyl chloride by distillation under reduced pressure

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: To a solution of 1.000 g of 9,12,15-octadecatrienoic acid in 20 ml of dry chloroform at room temperature was added in the atmosphere of argon 0.50 ml of oxalyl chloride. The mixture was reacted for 2 hours. From the reaction mixture were removed the chloroform and the remaining oxalyl chloride by distillation. The 9,12,15-octadecatrienoyl chloride thus produced was again dissolved in 2 ml of dry chloroform. The mixture was reacted for 2 hours From the reaction mixture were removed the chloroform the remaining oxalyl chloride by distillation