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CC(C(=O)C1=CC=CC=C1)OC製品情報
2-methoxy-1-phenylpropan-1-one (CAS 6493-83-0) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 11309701
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-d088da6206c14dafae911e4dfc3113b7反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-bca319399d9e428682e2822a23c5c97a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-e15b3a7003e045edadd4160fbd2aa37f反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-d088da6206c14dafae911e4dfc3113b7反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3) GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3) GC, tr 4.58 min
ソース ID: ord-12178347044140d0a94eeb3ca9a0b7db反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 ml) The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-e3dadd7477a64b48ba473891b0f5837e反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 ml) The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-e3dadd7477a64b48ba473891b0f5837e反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-bca319399d9e428682e2822a23c5c97a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-bca319399d9e428682e2822a23c5c97a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-e15b3a7003e045edadd4160fbd2aa37f反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:1% IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-e15b3a7003e045edadd4160fbd2aa37f反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 2-hydroxypropiophenone (3.00 g, 20.0 mmol), iodomethane (3.40 g, 24.0 mmol), and K2CO3 (granular, anh.; 13.8 g, 99.9 mmol) was refluxed in acetone (75 mL) for 18 h. The reaction mixture was cooled to room temperature and the inorganic salts were removed by filtration. The filtrate was evaporated under vacuum to give an oil which was subsequently dissolved in diethyl ether (200 mL) and then washed with 0.1N NaOH (3×50 mL) followed by H2O (50 mL). The organic layer was dried (anh. Na2SO4), filtered, and evaporated to an orange oil (3.17 g, 96.9%). This material was used in the following step without further purification. TLC, Rf 0.55 (1% MeOH:l % IPA:CHCl3); GC, tr 4.58 min; MS, m/z 164 (M+1). the inorganic salts were removed by filtration The filtrate was evaporated under vacuum to give an oil which washed with 0.1N NaOH (3×50 mL) The organic layer was dried (anh. Na2SO4) filtered evaporated to an orange oil (3.17 g, 96.9%) This material was used in the following step without further purification tr 4.58 min
ソース ID: ord-cbdb9df44d244fdc8371bcf42b84aa10PubChem References
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