反応 #1244659
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US09018175B2
反応条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of propoxyacetonitrile (3.03 g) and hydroxylamine (2.01 g, 50 wt % in water) is stirred for 2 h at 100° C. At RT DCM is added, the organic phase is separated, dried over sodium sulfate and concentrated under reduced pressure to give the title compound as an oil. the organic phase is separated dried over sodium sulfate concentrated under reduced pressure
ソース ID: ord-1489afd5ce5c4c1e95fdd821af9fbff7