1-chloroethylbenzene

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.01; pressure:0.00; stir:

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: Using a procedure analogous to that of Example 1, 100 g (0.82 mol) of 1-phenylethane-1-ol is reacted with 97.6 g (0.529 mol) of cyanuric chloride over a period of 14 hours at a reaction temperature of 90° C. After phase separation, treatment with sodium hydroxide and purification by distillation, 1-chloro-1-phenylethane having a purity of>99% and containing<0.3% of isomeric alkyl chlorides is obtained. After phase separation, treatment with sodium hydroxide and purification by distillation, 1-chloro-1-phenylethane having a purity of>99% containing<0.3% of isomeric alkyl chlorides is obtained