azane;2-dodecoxyethyl hydrogen sulfate

反応条件: temp:74.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: For Examples I-XV, about one-third to all of the total alkyl sulfate surfactant (ammonium laureth-3 sulfate (added as a 26% solution) and/or ammonium lauryl sulfate (added as a 25% solution)) is added to a jacketed mix tank and heated to about 74° C. with slow agitation to form a surfactant solution. Sodium sulfate and fatty alcohol, as applicable, are added to the tank and allowed to disperse. Ethylene glycol distearate (EGDS) is then added to the mixing vessel, and melted. After the EGDS is well dispersed (usually about 5 to 20 minutes) polyethylene glycol and the preservative, if used are added and mixed into the surfactant solution. This mixture is passed through a heat exchanger where it is cooled to about 35° C. and collected in a finishing tank. As a result of this cooling step, the ethylene glycol distearate crystallizes to form a crystalline network in the product. The remainder of the ammonium laureth sulfate, lauryl sulfate and other ingredients including the silicone premix, if included in the formula, are added to the finishing tank with ample agitation to insure a homogeneous mixture. A sufficient amount of the silicone premix is added to provide the desired level of dimethicone in the final product Polyquaternium 10, if added, is typically dispersed in water as a 0 1% solution before addition to the final mix. Once all ingredients have been added, ammonium xylene sulfonate or additional sodium sulfate can be added to the mixture to thin or thicken respectively to achieve a desired product viscosity. Preferred viscosities range from about 2500 to about 6000 cS at 25° C. (as measured by a Wells-Brookfield cone and plate viscometer at 15/s). is added to a jacketed mix tank to form a surfactant solution to disperse the preservative, if used are added mixed into the surfactant solution is cooled to about 35° C. collected in a finishing tank As a result of this cooling step the ethylene glycol distearate crystallizes to form a crystalline network in the product premix are added to the finishing tank with ample agitation is added

反応条件: temp:74.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: For Examples I-XV, about one-third to all of the total alkyl sulfate surfactant (ammonium laureth-3 sulfate (added as a 26% solution) and/or ammonium lauryl sulfate (added as a 25% solution)) is added to a jacketed mix tank and heated to about 74° C. with slow agitation to form a surfactant solution. Sodium sulfate and fatty alcohol, as applicable, are added to the tank and allowed to disperse. Ethylene glycol distearate (EGDS) is then added to the mixing vessel, and melted. After the EGDS is well dispersed (usually about 5 to 20 minutes) polyethylene glycol and the preservative, if used are added and mixed into the surfactant solution. This mixture is passed through a heat exchanger where it is cooled to about 35° C. and collected in a finishing tank. As a result of this cooling step, the ethylene glycol distearate crystallizes to form a crystalline network in the product. The remainder of the ammonium laureth sulfate, lauryl sulfate and other ingredients including the silicone premix, if included in the formula, are added to the finishing tank with ample agitation to insure a homogeneous mixture. A sufficient amount of the silicone premix is added to provide the desired level of dimethicone in the final product Polyquaternium 10, if added, is typically dispersed in water as a 0 1% solution before addition to the final mix. Once all ingredients have been added, ammonium xylene sulfonate or additional sodium sulfate can be added to the mixture to thin or thicken respectively to achieve a desired product viscosity. Preferred viscosities range from about 2500 to about 6000 cS at 25° C. (as measured by a Wells-Brookfield cone and plate viscometer at 15/s). is added to a jacketed mix tank to form a surfactant solution to disperse the preservative, if used are added mixed into the surfactant solution is cooled to about 35° C. collected in a finishing tank As a result of this cooling step the ethylene glycol distearate crystallizes to form a crystalline network in the product premix are added to the finishing tank with ample agitation is added

反応条件: temp:68.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A styrene-butadiene dispersion was prepared by free-radical polymerization from 6 kg of styrene, 8.4 kg of 1,3-butadiene, 3.6 kg of acrylic acid, 0.41 kg of styrene seed latex dispersion (34% by weight in water, particle size about 30 to 35 nm), 135 g of Texapon® NSO solution (sodium lauryl ether sulfate having on average 2.5 ethylene oxide units; 28% strength by weight in water), 150 g of sodium hydroxide solution (10% strength by weight in water), 110 g of sodium peroxodisulfate and 18.28 kg of water at 82° C. Excess 1,3-butadiene was removed by injecting 2 bar of nitrogen with stirring into the dispersion, which had been cooled to 68° C., releasing the pressure and applying a slight underpressure (750 mbar absolute) and repeating this procedure in automated form about 1500 times. After 4 hours, a dispersion was obtained which had a solids content of 51.3% by weight, a pH of 4.8, and residual monomer contents of 1669 ppm of styrene and 280 ppm of acrylic acid. Excess 1,3-butadiene was removed a dispersion was obtained which

反応条件: temp:74.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: For Examples I-XV, about one-third to all of the total alkyl sulfate surfactant (ammonium laureth-3 sulfate (added as a 26% solution) and/or ammonium lauryl sulfate (added as a 25% solution)) is added to a jacketed mix tank and heated to about 74° C. with slow agitation to form a surfactant solution. Sodium sulfate and fatty alcohol, as applicable, are added to the tank and allowed to disperse. Ethylene glycol distearate (EGDS) is then added to the mixing vessel, and melted. After the EGDS is well dispersed (usually about 5 to 20 minutes) polyethylene glycol and the preservative, if used are added and mixed into the surfactant solution. This mixture is passed through a heat exchanger where it is cooled to about 35° C. and collected in a finishing tank. As a result of this cooling step, the ethylene glycol distearate crystallizes to form a crystalline network in the product. The remainder of the ammonium laureth sulfate, lauryl sulfate and other ingredients including the silicone premix, if included in the formula, are added to the finishing tank with ample agitation to insure a homogeneous mixture. A sufficient amount of the silicone premix is added to provide the desired level of dimethicone in the final product Polyquaternium 10, if added, is typically dispersed in water as a 0 1% solution before addition to the final mix. Once all ingredients have been added, ammonium xylene sulfonate or additional sodium sulfate can be added to the mixture to thin or thicken respectively to achieve a desired product viscosity. Preferred viscosities range from about 2500 to about 6000 cS at 25° C. (as measured by a Wells-Brookfield cone and plate viscometer at 15/s). is added to a jacketed mix tank to form a surfactant solution to disperse the preservative, if used are added mixed into the surfactant solution is cooled to about 35° C. collected in a finishing tank As a result of this cooling step the ethylene glycol distearate crystallizes to form a crystalline network in the product premix are added to the finishing tank with ample agitation is added

反応条件: temp:68.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A styrene-butadiene dispersion was prepared by free-radical polymerization from 6 kg of styrene, 8.4 kg of 1,3-butadiene, 3.6 kg of acrylic acid, 0.41 kg of styrene seed latex (34% by weight in water, particle size about 30 to 35 nm), 135 g of Texapon® NSO (sodium lauryl ether sulfate having on average 2.5 ethylene oxide units), 15 g of sodium hydroxide, 110 g of sodium peroxodisulfate and 18.28 kg of water at 82° C. Excess 1,3-butadiene was removed by injecting 2 bar of nitrogen into the dispersion, with stirring, after cooling the dispersion to 68° C., then releasing the dispersion from pressure and applying a slight underpressure (750 mbar absolute), and repeating this procedure in automated form about 1500 times. After 4 hours, a dispersion was obtained which had a solids content of 51.3% by weight, a pH of 4.8, and residual monomer contents of 1845 ppm of styrene and 280 ppm of acrylic acid. Excess 1,3-butadiene was removed a dispersion was obtained which

反応条件: temp:68.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A styrene-butadiene dispersion was prepared by free-radical polymerization from 6 kg of styrene, 8.4 kg of 1,3-butadiene, 3.6 kg of acrylic acid, 0.41 kg of styrene seed latex (34% by weight in water, particle size about 30 to 35 nm), 135 g of Texapon® NSO (sodium lauryl ether sulfate having on average 2.5 ethylene oxide units), 15 g of sodium hydroxide, 110 g of sodium peroxodisulfate and 18.28 kg of water at 82° C. Excess 1,3-butadiene was removed by injecting 2 bar of nitrogen into the dispersion, with stirring, after cooling the dispersion to 68° C., then releasing the dispersion from pressure and applying a slight underpressure (750 mbar absolute), and repeating this procedure in automated form about 1500 times. After 4 hours, a dispersion was obtained which had a solids content of 51.3% by weight, a pH of 4.8, and residual monomer contents of 1845 ppm of styrene and 280 ppm of acrylic acid. Excess 1,3-butadiene was removed a dispersion was obtained which

反応条件: temp:68.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A styrene-butadiene dispersion was prepared by free-radical polymerization from 6 kg of styrene, 8.4 kg of 1,3-butadiene, 3.6 kg of acrylic acid, 0.41 kg of styrene seed latex dispersion (34% by weight in water, particle size about 30 to 35 nm), 135 g of Texapon® NSO solution (sodium lauryl ether sulfate having on average 2.5 ethylene oxide units; 28% strength by weight in water), 150 g of sodium hydroxide solution (10% strength by weight in water), 110 g of sodium peroxodisulfate and 18.28 kg of water at 82° C. Excess 1,3-butadiene was removed by injecting 2 bar of nitrogen with stirring into the dispersion, which had been cooled to 68° C., releasing the pressure and applying a slight underpressure (750 mbar absolute) and repeating this procedure in automated form about 1500 times. After 4 hours, a dispersion was obtained which had a solids content of 51.3% by weight, a pH of 4.8, and residual monomer contents of 1669 ppm of styrene and 280 ppm of acrylic acid. Excess 1,3-butadiene was removed a dispersion was obtained which

反応条件: temp:74.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: For Examples I-XV, about one-third to all of the total alkyl sulfate surfactant (ammonium laureth-3 sulfate (added as a 26% solution) and/or ammonium lauryl sulfate (added as a 25% solution)) is added to a jacketed mix tank and heated to about 74° C. with slow agitation to form a surfactant solution. Sodium sulfate and fatty alcohol, as applicable, are added to the tank and allowed to disperse. Ethylene glycol distearate (EGDS) is then added to the mixing vessel, and melted. After the EGDS is well dispersed (usually about 5 to 20 minutes) polyethylene glycol and the preservative, if used are added and mixed into the surfactant solution. This mixture is passed through a heat exchanger where it is cooled to about 35° C. and collected in a finishing tank. As a result of this cooling step, the ethylene glycol distearate crystallizes to form a crystalline network in the product. The remainder of the ammonium laureth sulfate, lauryl sulfate and other ingredients including the silicone premix, if included in the formula, are added to the finishing tank with ample agitation to insure a homogeneous mixture. A sufficient amount of the silicone premix is added to provide the desired level of dimethicone in the final product Polyquaternium 10, if added, is typically dispersed in water as a 0 1% solution before addition to the final mix. Once all ingredients have been added, ammonium xylene sulfonate or additional sodium sulfate can be added to the mixture to thin or thicken respectively to achieve a desired product viscosity. Preferred viscosities range from about 2500 to about 6000 cS at 25° C. (as measured by a Wells-Brookfield cone and plate viscometer at 15/s). is added to a jacketed mix tank to form a surfactant solution to disperse the preservative, if used are added mixed into the surfactant solution is cooled to about 35° C. collected in a finishing tank As a result of this cooling step the ethylene glycol distearate crystallizes to form a crystalline network in the product premix are added to the finishing tank with ample agitation is added