01
反応 #4097592
反応式
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関連文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-77d92a7a05234497ae105853e1bbef8a2D 化学構造データベース ID 14518958
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SMILES
CNC(=O)CNCC(=O)NC——
製品情報
N-methyl-2-[[2-(methylamino)-2-oxoethyl]amino]acetamide
N-methyl-2-[[2-(methylamino)-2-oxoethyl]amino]acetamide (CAS 725686-07-7) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
CAS番号725686-07-7
データベース ID14518958
分子式—
更新日2023-01-08
想定用途
想定用途
専門的研究・工業用途限定
データベース ID 14518958
計算物性
精密質量—
XLogP—
トポロジカル極性表面積—
水素結合供与体—
水素結合受容体—
回転可能結合—
- IUPAC 名
- —
- InChIKey
- —
- SMILES
- CNC(=O)CNCC(=O)NC
- InChI
- —
安全上の注意
安全性と注記
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
関連反応
12 反応 · 12 文献
02
反応 #3231749
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07144911B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
ソース ID: ord-357458fff450461e85baad9d3568269703
反応 #2902795
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07531566B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 (br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 (br s 1H); MS (ESI) m/e 160 (M+H+) filtered concentrated in vacuo
ソース ID: ord-ae480de714cb48fda70d4bcd3524d6b104
反応 #2532779
反応式
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07737283B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79(d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
ソース ID: ord-d7989f36f09e446187dabeec80ee1ec105
反応 #2466000
反応式
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関連文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-77d92a7a05234497ae105853e1bbef8a06
反応 #2320282
反応式
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07737283B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79(d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
ソース ID: ord-d7989f36f09e446187dabeec80ee1ec107
反応 #1210459
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07666895B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 (br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 (br s 1H); MS (ESI) m/e 160 (M+H+) filtered concentrated in vacuo
ソース ID: ord-c4d9a121559f472e987a0ee80953a77e08
反応 #1074247
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07202257B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 )br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 )br s 1H); MS (ESI) m/e 160 )M+H+). filtered concentrated in vacuo
ソース ID: ord-fd06343229954c3f9c663fa1444f8be209
反応 #1021444
反応式
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関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07279576B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of 2-(benzyl-methylcarbamoylmethyl-amino)N-methyl-acetamid (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-methyl-2-(methylcarbamoylmethyl-amino)-acetamide in quantitative yield (1.76 g). 1HNMR(CDCl3) δ 6.95(brs, 2H), 3.23(s, 4H), 2.79(d, J=4.8 Hz, 6H), 2.25(brs, 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
ソース ID: ord-f9b9c85b6c9c4e33af164179c2f64ed610
反応 #763755
反応式
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07144911B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
ソース ID: ord-357458fff450461e85baad9d3568269711
反応 #433402
反応式
表示可能な構造データがありません
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07531566B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95 (br s, 2H), 3.23 (s, 4H), 2.79 (d, J=6.0, 4.8 Hz), 2.25 (br s 1H); MS (ESI) m/e 160 (M+H+) filtered concentrated in vacuo
ソース ID: ord-ae480de714cb48fda70d4bcd3524d6b112
反応 #78866
反応式
表示可能な構造データがありません
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表示可能な構造データがありません
関連文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07737283B2
反応条件: temp:40.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: The mixture of N-(2-methylamino-2-oxoethyl)-N-(phenylmethyl)-glycine methylamide (3.09 g, 11.2 mmol) in MeOH (30 mL) was added 10% Pd/C (0.15 g). The mixture was stirred and heated to 40° C. under 40 psi H2 for 10 h, filtered and concentrated in vacuo to yield N-(2-methylamino-2-oxoethyl)-glycine methylamide in quantitative yield (1.76 g). 1H NMR (CDCl3): δ 6.95(br s, 2H), 3.23 (s, 4H), 2.79(d, J=6.0, 4.8 Hz), 2.25(br s 1H); MS (ESI) m/e 160(M+H+) filtered concentrated in vacuo
ソース ID: ord-d7989f36f09e446187dabeec80ee1ec1PubChem References
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CAS 725686-07-7N-methyl-2-[[2-(methylamino)-2-oxoethyl]amino]acetamide
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