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C1(=C(C(=C(C(=C1F)F)F)F)F)C(=O)C2=C(C(=C(C(=C2F)F)F)F)F製品情報
Decafluorobenzophenone (CAS 853-39-4) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 70068
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
9 反応 · 9 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-910ecba8b4d1406d9ad567b318242d81反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-a5294303fdcc4562a1bcd0a97cbe79d7反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-a5294303fdcc4562a1bcd0a97cbe79d7反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-9797598e0f8945dcacc0fb81a52e30ac反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-a5294303fdcc4562a1bcd0a97cbe79d7反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-910ecba8b4d1406d9ad567b318242d81反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-c84ac2dbbfd3438ea54fd87743b97984反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-9797598e0f8945dcacc0fb81a52e30ac反応条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 4.9 g of decafluorobenzophenone and 2.7 g of trichloroacetic acid was added to 15 mL of hexamethylphosphoramide. The stirred reaction mixture was maintained at about 0° C. for about 2 hours and then allowed to warm to room temperature and continue stirring at ambient temperature for the next 15 hours. The reaction mixture was characterized by GC and fluorine NMR to show a conversion of approximately 20% to the desired carbinol. This carbinol can be converted to the corresponding acrylate by methods previously described (cf. Example 24). The stirred reaction mixture to warm to room temperature
ソース ID: ord-a5294303fdcc4562a1bcd0a97cbe79d7PubChem References
化合物の公開データベース記録に掲載された情報源です。