1-(aminomethyl)-4,4-dimethylcyclohexan-1-ol

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A mixture of 4,4-dimethyl-1-(nitromethyl)cyclohexanol (1.5 g, 0.0072 mol) and palladium hydroxide (0.1 g, 0.0001 mol) in methanol (50 mL, 1 mol) was stirred under hydrogen (1 atm) at room temperature overnight. The mixture was filtered and concentrated to afford the desired product as a clear oil. (1.08 g, 95%). The mixture was filtered concentrated

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A mixture of 4,4-dimethyl-1-(nitromethyl)cyclohexanol (1.5 g, 0.0072 mol) and palladium hydroxide (0.1 g, 0.0001 mol) in methanol (50 mL, 1 mol) was stirred under hydrogen (1 atm) at room temperature overnight. The mixture was filtered and concentrated to afford the desired product as a clear oil. (1.08 g, 95%). The mixture was filtered concentrated

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A mixture of 4,4-dimethyl-1-(nitromethyl)cyclohexanol (1.5 g, 0.0072 mol) and palladium hydroxide (0.1 g, 0.0001 mol) in methanol (50 mL, 1 mol) was stirred under hydrogen (1 atm) at room temperature overnight. The mixture was filtered and concentrated to afford the desired product as a clear oil. (1.08 g, 95%). The mixture was filtered concentrated

反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

実験手順: A mixture of 4,4-dimethyl-1-(nitromethyl)cyclohexanol (1.5 g, 0.0072 mol) and palladium hydroxide (0.1 g, 0.0001 mol) in methanol (50 mL, 1 mol) was stirred under hydrogen (1 atm) at room temperature overnight. The mixture was filtered and concentrated to afford the desired product as a clear oil. (1.08 g, 95%). The mixture was filtered concentrated