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CCNC(=O)NC1=CC=C(C=C1)N製品情報
1-(4-aminophenyl)-3-ethylurea (CAS 70826-92-5) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
想定用途
専門的研究・工業用途限定
データベース ID 22061027
安全上の注意
For professional research and industrial use only. Review the supplier safety data sheet before handling.
合成データ
12 反応 · 12 文献
反応条件: temp:0.00; pressure:0.00; stir:
ソース ID: ord-062c28e54830457db40378ca5ec2ba31反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-8a04fcb0539a4b49908fcbcc9a29de4a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-f2d348960ee1453093dc4134bd061292反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-64ddba5364244c09b7b73746c4e040fa反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-64ddba5364244c09b7b73746c4e040fa反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-1421dcd4d32c45fa8f7913e99de0ccc4反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-52fab92f894c40e7824e159c80a37c18反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-52fab92f894c40e7824e159c80a37c18反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-68863a5a5c6c4048b0d2e0b15e791e48反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-8a04fcb0539a4b49908fcbcc9a29de4a反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-5fa56e27b3d64b99beeac163c91b4abc反応条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
実験手順: A mixture of 1,4-diaminobenzene (4 g, 37 mmol), ethyl isocyanate (1 mL, 12.6 mmol) and potassium carbonate (8.72 g, 63 mmol) in THF (20 mL) was stirred at room temperature overnight. The reaction mixture was partitioned in 1N HCl solution (80 mL) and ethyl acetate (80 mL). The aqueous layer was extracted with ethyl acetate (4×80 mL). The combined organic layers was dried, evaporated, recrystallized from MeOH/CH2Cl2/hexanes to give 4-(ethylaminocarbonylamino)aniline (1.4 g, 62%) as a beige solid. The reaction mixture was partitioned in 1N HCl solution (80 mL) The aqueous layer was extracted with ethyl acetate (4×80 mL) The combined organic layers was dried evaporated recrystallized from MeOH/CH2Cl2/hexanes
ソース ID: ord-5fa56e27b3d64b99beeac163c91b4abcPubChem References
化合物の公開データベース記録に掲載された情報源です。
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